N,O-双三甲硅基乙酰胺合成路线 (共 163 条)
反应条件
sodium in N,N,N',N',N'',N''-hexamethylphosphoric triamide Ambient temperature; Yield given. Yields of byproduct given;
参考文献
Dedier, James; Gerval, Pierre; Frainnet, Emile
Journal of Organometallic Chemistry, 1980 , vol. 185, # 2 p. 183 - 198
反应条件
sodium in N,N,N',N',N'',N''-hexamethylphosphoric triamide Ambient temperature; Yield given. Yields of byproduct given;
参考文献
Dedier, James; Gerval, Pierre; Frainnet, Emile
Journal of Organometallic Chemistry, 1980 , vol. 185, # 2 p. 183 - 198
反应条件
sodium in N,N,N',N',N'',N''-hexamethylphosphoric triamide Ambient temperature; Yield given. Yields of byproduct given;
参考文献
Dedier, James; Gerval, Pierre; Frainnet, Emile
Journal of Organometallic Chemistry, 1980 , vol. 185, # 2 p. 183 - 198
反应条件
in deuterated toluene
参考文献
Nemoto, Tetsuhiro; Masuda, Takamasa; Matsumoto, Takayoshi; Hamada, Yasumasa
Journal of Organic Chemistry, 2005 , vol. 70, # 18 p. 7172 - 7178
反应条件
bis(η3-allyl-μ-chloropalladium(II)); (5S,2'R)-4,5-dihydro-2-(2'-diphenylphosphino-2'-phenylethyl)-5-tert-butyl-1,3-oxazole; tetrahexylammonium fluoride in acetonitrile Ambient temperatureother reactant: 2-cyclopentenyl acetate, other reagents: other chiral phosphine-oxazoline ligands/<Pd(η3-C3H5)Cl>2/nBu4NF or nHex4NF or nHex4NBr or TBAOAc or KOAc, NaH presence, other solvents: CH2Cl2, C6H6, THF, other temperature; MechanismProduct distribution;
参考文献
Gilbertson, Scott R.; Chang, Cheng-Wei T.
Journal of Organic Chemistry, 1998 , vol. 63, # 23 p. 8424 - 8431
反应条件
sodium in N,N,N',N',N'',N''-hexamethylphosphoric triamide Ambient temperature;
参考文献
Dedier, James; Gerval, Pierre; Frainnet, Emile
Journal of Organometallic Chemistry, 1980 , vol. 185, # 2 p. 183 - 198
反应条件
in acetonitrile 1 h; Ambient temperature;
参考文献
Rajeswari, Sundaramoorthi; Jones, Robert J.; Cava, Michael P.
Tetrahedron Letters, 1987 , vol. 28, # 43 p. 5099 - 5102
参考文献
White,E. et al.
Journal of Organic Chemistry, 1970 , vol. 35, p. 4241 - 4244
反应条件
methanol 1.) 35-40 deg C, 2 h, 2.) 0 deg C; Yield given. Multistep reaction;
参考文献
Gonda, Josef; Antalova, Zuzana
Collection of Czechoslovak Chemical Communications, 1991 , vol. 56, # 3 p. 685 - 694
反应条件
in acetonitrile Ambient temperature;
参考文献
Steffens, Ralph; Leumann, Christian
Helvetica Chimica Acta, 1997 , vol. 80, # 8 p. 2426 - 2439