氢化物三(三甲基甲硅烷基)锗合成路线 (共 12 条)
反应条件
1: diethyl ether; hexane
2: diethyl ether
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参考文献
Nanjo, Masato; Oda, Takashi; Mochida, Kunio
Bulletin of the Chemical Society of Japan, 2003 , vol. 76, # 6 p. 1261 - 1264
反应条件
With tetrachloromethane in Petroleum ether; pentane under Ar; soln. of Ge-compd./petroleum ether added slowly to CCl4/pentane at 0°C, mixt. stirred overnight; evapn. (reduced pressure), sublimation at 25°C/6E-5 torr, elem. anal.;
参考文献
Brook, A. G.; Abdesaken, F.; Soellradl, H. Journal of Organometallic Chemistry, 1986 , vol. 299, p. 9 - 14