(S)-(-)-1-(1-萘基)乙胺合成路线 （共 41 条）
反应条件
heptakis-(6-O-TIPS)-β-CD; triethylamine in cyclohexane T=10°C; 6 h; Resolution of racemate; Reagent/catalystSolventTime; enantioselective reaction;
参考文献
Tetrahedron, , vol. 70, # 2 p. 197 - 203
反应条件
heptakis-(6-O-TIPS)-β-CD; triethylamine in cyclohexane T=10°C; 6 h; Resolution of racemate; enantioselective reaction;
参考文献
Tetrahedron, , vol. 70, # 2 p. 197 - 203
反应条件
heptakis-(6-O-TIPS)-β-CD; triethylamine in cyclohexane T=10°C; 6 h; Resolution of racemate; enantioselective reaction;
参考文献
Tetrahedron, , vol. 70, # 2 p. 197 - 203
反应条件
1: chiral 1,1'-bisphosphanoferrocene; H2 / {Ir(cod)Cl}2 / CH2Cl2 / 20 °C / 51714.8 Torr 2: CAN / methanol; H2O View Scheme
参考文献
Angewandte Chemie - International Edition, , vol. 40, # 18 p. 3425 - 3428
反应条件
1: With [((R)-tol-binap)RuCl2(DMF)x]; ammonia; ammonium formate in methanol T=85°C; Leuckart-Wallach reaction; 30 h; 2: With hydrogenchloride in ethanol 1 h; Heating; Title compound not separated from byproducts;
参考文献
Angewandte Chemie - International Edition, , vol. 42, # 44 p. 5472 - 5474
反应条件
Candida antarctica lipase B in n-heptane T=80°C; 25 h;
参考文献
Nechab, Malek; Azzi, Nadia; Vanthuyne, Nicolas; Bertrand, Michele; Gastaldi, Stephane; Gil, Gerard
Journal of Organic Chemistry, 2007 , vol. 72, # 18 p. 6918 - 6923
反应条件
CF3COOH in dichloromethane To a soln. of complex in CH2Cl2 was added CF3CO2H, the mixt. was stirred for 10 min (N2 atm.); evapd., extd. with H2O, NaBF4 was added;; ppt. was filtered, recrystd. from CH2Cl2-hexane;;
参考文献
Merrifield, James H.; Strouse, Charles E.; Gladysz, J. A.
Organometallics, 1982 , vol. 1, p. 1204 - 1211
反应条件
1: 74.9 percent / H2, conc. ammonia / Raney nickel / aq. ethanol / 24 h / 3040 Torr / Ambient temperature View Scheme
参考文献
Tetrahedron, , vol. 50, # 34 p. 10309 - 10320
反应条件
Candida antarctica lipase in di-isopropyl ether T=30°C; 120 h;
参考文献
Yang, Bo; Zhang, Yanjun; Zhang, Shusheng; Izumi
Indian Journal of Chemistry - Section B Organic and Medicinal Chemistry, 2005 , vol. 44, # 6 p. 1312 - 1316
反应条件
Candida antarctica lipase in di-isopropyl ether T=30°C; 120 h;
参考文献
Yang, Bo; Zhang, Yanjun; Zhang, Shusheng; Izumi
Indian Journal of Chemistry - Section B Organic and Medicinal Chemistry, 2005 , vol. 44, # 6 p. 1312 - 1316
