1: 2-cyclohexylidene-1,1-dimethylhydrazine With n-butyllithium in tetrahydrofuran; hexane
T=0°C; 0.5 h;
2: (3-iodoprop-1-yl)benzene in tetrahydrofuran; hexane
T=0 - 25°C;
3: With sulfuric acid in tetrahydrofuran; hexane
T=25°C; 1 h; Further stages.;
参考文献
Wrobleski; Aube
Journal of Organic Chemistry, 2001 , vol. 66, # 3 p. 886 - 889
