双(二丁基氯基锡(四))氧化物合成路线 （共 19 条）
反应条件
in dichloromethane; water soln. of Bu2SnCl2 in CH2Cl2 was added to deionized water and mixed vigorously until pH reached 1.3; org. layer sepd., dried over Na2SO4; evapd.; recrystallized from t-amyl alcohol; elem. anal.;
参考文献
Journal of Organometallic Chemistry, , vol. 620, # 1-2 p. 211 - 226
反应条件
in tetrachloromethane equimolar amt. of PhCOCl and oligomer in CCl4 mixing and heating under reflux for 30 min, then treating with HCl gas; identified by m.p.;
参考文献
Journal of Organometallic Chemistry, , vol. 251, # 2 p. 203 - 208
反应条件
water in water; acetone byproducts: CH3CH=CH2; pptn.;
参考文献
Inorganica Chimica Acta, , vol. 24, p. L47
反应条件
ozone in tetrachloromethane passing of ozone (2-5 vol-percent on O2 stream) though soln. (20°C), pptn.;
参考文献
Journal of General Chemistry USSR (English Translation), , vol. 50, p. 1861 - 1863
Zhurnal Obshchei Khimii, , vol. 50, p. 2298 - 2300
反应条件
water in not given byproducts: 2,3-dimethyl-5-hexen-3-ol; stirring equimolar amts. (7 h), distn. (1 Torr), pptn. on addn. of H2O;
参考文献
Inorganica Chimica Acta, , vol. 24, p. L47
反应条件
ozone in hexane passing of ozone (2-5 vol-percent on O2 stream) though soln. (-78°C), pptn.; washing (-78°C);
参考文献
Journal of General Chemistry USSR (English Translation), , vol. 50, p. 1861 - 1863
Zhurnal Obshchei Khimii, , vol. 50, p. 2298 - 2300
反应条件
1: benzene 2: toluene 3: tetrachloromethane View Scheme
参考文献
Journal of Organometallic Chemistry, , vol. 251, # 2 p. 203 - 208
反应条件
1: toluene 2: tetrachloromethane View Scheme
参考文献
Journal of Organometallic Chemistry, , vol. 251, # 2 p. 203 - 208
反应条件
in benzene equimolar ratio of compounds; refluxing in benzene for ca. 3 h;; solvent removed (vacuum); treatment with MeCN to yield 1,3-dichlorotetrabutyldistannoxane as insoluble portion; evapn. of washing gave arsenic compound;
参考文献
Inorganica Chimica Acta, , vol. 144, p. 259 - 264
反应条件
equimolar ratio of compounds;;
参考文献
Inorganica Chimica Acta, , vol. 144, p. 259 - 264
