乙基 3-[4-(苄氧基)苯基]丙烯酸酯合成路线 （共 15 条）
反应条件
potassium hydroxide in tetrahydrofuran T=25°C; Wittig reaction; 12 h;
参考文献
Nicolaou; Boddy, Christopher N. C.; Li, Hui; Koumbis, Alexandros E.; Hughes, Robert; Natarajan, Swaminathan; Jain, Nareshkumar F.; Ramanjulu, Joshi M.; Braese, Stefan; Solomon, Michael E.
Chemistry - A European Journal, 1999 , vol. 5, # 9 p. 2602 - 2621
反应条件
in water T=90°C; 2 h; Inert atmosphere; optical yield given as percent de;
参考文献
Dethe, Dattatraya H.; Ranjan, Alok
RSC Advances, 2013 , vol. 3, # 45 p. 23692 - 23703
反应条件
pyrrolidine; (E,Z)-crotononitrile; ruthenium(II)-carbonyl-tris(triphenylphosphine) dihydride; 9,9-dimethyl-4,5-bis(diphenyl-phosphino)xanthene in toluene 2 h; Inert atmosphereReflux;
参考文献
Hall, Michael I.; Pridmore, Simon J.; Williams, Jonathan M. J.
Advanced Synthesis and Catalysis, 2008 , vol. 350, # 13 p. 1975 - 1978
反应条件
in dichloromethane T=20°C; Wittig olefination; 24 h;
参考文献
Reddy, S. Hari Krishna; Lee, Stephen; Datta, Apurba; Georg, Gunda I.
Journal of Organic Chemistry, 2001 , vol. 66, # 24 p. 8211 - 8214
反应条件
1: potassium carbonate / N,N-dimethyl-formamide / 12 h / 0 - 60 °C / Inert atmosphere 2: toluene / 4 h / Inert atmosphere; Reflux View Scheme
参考文献
Tetrahedron Letters, , vol. 52, # 48 p. 6366 - 6369
参考文献
Tao, Junhua; Hu, Shanghui; Pacholec, Michelle; Walsh, Christopher T.
Organic Letters, 2003 , vol. 5, # 18 p. 3233 - 3236
反应条件
1: 98 percent / K2CO3; KI / dimethylformamide / 12 h / 25 °C 2: 95 percent / KOH / tetrahydrofuran / 12 h / 25 °C View Scheme
参考文献
Angewandte Chemie - International Edition, , vol. 37, # 19 p. 2708 - 2714
反应条件
tris-(2-chloro-ethyl)-amine; triphenylphosphine; diethylazodicarboxylate in benzene 3 h; 0 deg C to RT;
参考文献
Tetrahedron Letters, , vol. 34, # 44 p. 7085 - 7088
反应条件
1: Zn / diethyl ether; benzene / 1 h / Heating 2: PCC / CH2Cl2 / 4 h / Ambient temperature 3: LiBH4, N,N'-dibenzoyl-D-cystine / 2-methyl-propan-2-ol; tetrahydrofuran / 5 h / -78 °C 4: 5 percent / HN3, DEAD, PPh3 / benzene / 3 h / 0 deg C to RT View Scheme
参考文献
Tetrahedron Letters, , vol. 34, # 44 p. 7085 - 7088
反应条件
1: LiBH4, N,N'-dibenzoyl-D-cystine / 2-methyl-propan-2-ol; tetrahydrofuran / 5 h / -78 °C 2: 5 percent / HN3, DEAD, PPh3 / benzene / 3 h / 0 deg C to RT View Scheme
参考文献
Tetrahedron Letters, , vol. 34, # 44 p. 7085 - 7088
