乙基 3-[4-(苄氧基)苯基]丙烯酸酯合成路线 （共 15 条）
反应条件
1: PCC / CH2Cl2 / 4 h / Ambient temperature 2: LiBH4, N,N'-dibenzoyl-D-cystine / 2-methyl-propan-2-ol; tetrahydrofuran / 5 h / -78 °C 3: 5 percent / HN3, DEAD, PPh3 / benzene / 3 h / 0 deg C to RT View Scheme
参考文献
Tetrahedron Letters, , vol. 34, # 44 p. 7085 - 7088
反应条件
1: With lithium borohydride in tetrahydrofuran T=20°C; 36 h; Inert atmosphere; 2: With ammonium chloride in tetrahydrofuran Inert atmosphere;
参考文献
Das, Biswanath; Suneel, Kanaparthy; Satyalakshmi, Gandham; Kumar, Duddukuri Nandan
Tetrahedron Asymmetry, 2009 , vol. 20, # 13 p. 1536 - 1540
反应条件
sodium hydroxide in ethanol; water T=60°C;
参考文献
Rokade, Balaji V.; Prabhu, Kandikere Ramaiah
Organic and Biomolecular Chemistry, 2013 , vol. 11, # 39 p. 6713 - 6716
反应条件
1: sodium hydroxide / ethanol; water / 60 °C 2: copper(l) chloride; tert.-butylnitrite / acetonitrile / 80 °C View Scheme
参考文献
Rokade, Balaji V.; Prabhu, Kandikere Ramaiah
Organic and Biomolecular Chemistry, 2013 , vol. 11, # 39 p. 6713 - 6716
反应条件
1.1: K2[OsO2(OH)4]; LiOH*H2O; (DHQ)2PHAL / 2-methyl-propan-2-ol; H2O; acetonitrile / 24 h / 0 - 5 °C
1.2: HCl / ethanol / 4 h / 90 °C
2.1: 23 g / NaHCO3 / tetrahydrofuran / 5 h / 20 °C
3.1: 75 percent / PPTS / toluene / 8 h / 90 °C
View Scheme
参考文献
Reddy, S. Hari Krishna; Lee, Stephen; Datta, Apurba; Georg, Gunda I.
Journal of Organic Chemistry, 2001 , vol. 66, # 24 p. 8211 - 8214
