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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
1043421-43-7
合成路线
(共 6 条)
1043421-43-7
→
反应条件
98130-56-4
2-溴-4,6-二氟苯酚
反应条件
1: sulfuric acid / acetic acid / 1 h / 100 °C 2: sodium hypochlorite; sodium hydroxide / methanol / 24 h / 25 °C 3: hydrogen / methanol / 20 h / 80 °C / 22502.3 Torr 4: water; potassium hydroxide / methanol / 24 h / Reflux 5: bromine / water / 2 h / 0 - 5 °C View Scheme
参考文献
Beliaev, Alexandre; Wahnon, Jorge; Russo, Domenico
Organic Process Research and Development, 2012 , vol. 16, # 4 p. 704 - 709
1043421-43-7
→
反应条件
1034001-13-2
反应条件
1: sulfuric acid / acetic acid / 1 h / 100 °C 2: sodium hypochlorite; sodium hydroxide / methanol / 24 h / 25 °C View Scheme
参考文献
Organic Process Research and Development, , vol. 16, # 4 p. 704 - 709
1043421-43-7
→
反应条件
760173-05-5
(R)-5-(2-氨基乙基)-1-(6,8-二氟苯并二氢吡喃-3-基)-1,3-二氢咪唑-2-硫酮
反应条件
1: sulfuric acid / acetic acid / 1 h / 100 °C 2: sodium hypochlorite; sodium hydroxide / methanol / 24 h / 25 °C 3: hydrogen / methanol / 20 h / 80 °C / 22502.3 Torr 4: water; potassium hydroxide / methanol / 24 h / Reflux 5: ethanol; water / 1 h / 20 °C 6: acetic acid / 2 - 4 h / 100 °C 7: sodium tetrahydroborate / dichloromethane; water; isopropyl alcohol / 16 h / 20 - 25 °C View Scheme
参考文献
Beliaev, Alexandre; Wahnon, Jorge; Russo, Domenico
Organic Process Research and Development, 2012 , vol. 16, # 4 p. 704 - 709
1043421-43-7
→
反应条件
1044596-95-3
反应条件
Multi-step reaction with 6 steps 1: sulfuric acid / acetic acid / 1 h / 100 °C2: sodium hypochlorite; sodium hydroxide / methanol / 24 h / 25 °C3: hydrogen / methanol / 20 h / 80 °C / 22502.3 Torr4: water; potassium hydroxide / methanol / 24 h / Reflux5: ethanol; water / 1 h / 20 °C6: acetic acid / 2 - 4 h / 100 °C
参考文献
Beliaev, Alexandre; Wahnon, Jorge; Russo, Domenico Organic Process Research and Development, 2012 , vol. 16, # 4 p. 704 - 709
1043421-43-7
→
反应条件
1044597-03-6
反应条件
Multi-step reaction with 5 steps 1: sulfuric acid / acetic acid / 1 h / 100 °C2: sodium hypochlorite; sodium hydroxide / methanol / 24 h / 25 °C3: hydrogen / methanol / 20 h / 80 °C / 22502.3 Torr4: water; potassium hydroxide / methanol / 24 h / Reflux5: ethanol; water / 1 h / 20 °C
参考文献
Beliaev, Alexandre; Wahnon, Jorge; Russo, Domenico Organic Process Research and Development, 2012 , vol. 16, # 4 p. 704 - 709
1043421-43-7
→
反应条件
1151797-94-2
反应条件
With sulfuric acid in acetic acid T=100°C; 1 h;
参考文献
Beliaev, Alexandre; Wahnon, Jorge; Russo, Domenico Organic Process Research and Development, 2012 , vol. 16, # 4 p. 704 - 709