反应条件
1: trifluoroacetic acid / dichloromethane / 0 - 20 °C
2: benzotriazol-1-ol; N-ethyl-N,N-diisopropylamine; HATU / dichloromethane; acetonitrile
3: triethylsilane; trifluoroacetic anhydride / 2 h / 0 - 20 °C
4: triethylamine / dichloromethane / 3 h / 0 - 20 °C
View Scheme
参考文献
Benelkebir, Hanae; Marie, Sabrina; Hayden, Annette L.; Lyle, Jason; Loadman, Paul M.; Crabb, Simon J.; Packham, Graham; Ganesan
Bioorganic and Medicinal Chemistry, 2011 , vol. 19, # 12 p. 3650 - 3658
