(S)-(+)-2-甲基丁酯甲磺酸合成路线 (共 5 条)
反应条件
triethylamine in dichloromethane 0.333333 h;
参考文献
Brookhart, Maurice; Liu, Yumin; Goldman, Emma W.; Timmers, Debra A.; Williams, Gregory D.
Journal of the American Chemical Society, 1991 , vol. 113, # 3 p. 927 - 939
反应条件
1: LiAlH4 / diethyl ether / 16 h / 40 °C 2: Et3N / CH2Cl2 / 1 h / -10 °C View Scheme
参考文献
Journal of Natural Products, , vol. 67, # 8 p. 1277 - 1282
反应条件
lithium bromide in acetone 2 h; Heating;
参考文献
Allmendinger, Thomas
Tetrahedron, 1991 , vol. 47, # 27 p. 4905 - 4914
反应条件
1: 77 percent / various solvent(s) / 0.83 h / 120 - 180 °C 2: 45 percent / DIBAH / hexane; pentane / 0.5 h / -70 °C View Scheme
参考文献
Tietze, Lutz F.; Schiemann, Kai; Wegner, Christoph; Wulff, Christian
Chemistry--A European Journal, 1996 , vol. 2, # 9 p. 1164 - 1172
反应条件
sodium iodide in acetone Finkelstein reaction; Reflux;
参考文献
Richman, Jack E.
Tetrahedron Letters, 2010 , vol. 51, # 21 p. 2793 - 2796