hydrogen; palladium on activated charcoal in tetrahydrofuran P=2585.7 Torr; 0.583333 h;

1: 85 percent / H2 / 10percent Pd/C / tetrahydrofuran / 0.58 h / 2585.7 Torr 2: 95 percent / aq. LiOH / tetrahydrofuran; methanol / 6 h / 60 °C View Scheme

sodium periodate in tetrahydrofuran; water 2 h; Ambient temperature;