N-环己基-2-苯并噁唑胺合成路线 （共 11 条）
反应条件
tert.-butylhydroperoxide; tetra-(n-butyl)ammonium iodide; acetic acid in water; 1,2-dichloro-ethane T=90°C; 12 h; Green chemistry;
参考文献
Wang, Rui; Liu, Hong; Yue, Liang; Zhang, Xiao-Ke; Tan, Qiu-Yuan; Pan, Ruo-Lin
Tetrahedron Letters, 2014 , vol. 55, # 14 p. 2233 - 2237
反应条件
tetrakis(triphenylphosphine) palladium(0) in 1,4-dioxane T=20°C; 2 h;
参考文献
Liu, Bifu; Yin, Meizhou; Gao, Hanling; Wu, Wanqing; Jiang, Huanfeng
Journal of Organic Chemistry, 2013 , vol. 78, # 7 p. 3009 - 3020
反应条件
tert.-butylhydroperoxide; tetra-(n-butyl)ammonium iodide; acetic acid in water; acetonitrile T=80°C; 1 h; Inert atmosphere;
参考文献
Kloeckner, Ulrich; Weckenmann, Nicole M.; Nachtsheim, Boris J.
Synlett, 2012 , # 1 art. no. D23611ST, p. 97 - 100
反应条件
1: With acetic acid in chloroform T=60°C; 16 h; Inert atmosphere; 2: With sodium hydroxide in chloroform; water T=20°C; Inert atmosphere;
参考文献
Cioffi, Christopher L.; Lansing, John J.; Yueksel, Hamza
Journal of Organic Chemistry, 2010 , vol. 75, # 22 p. 7942 - 7945
反应条件
1,8-diazabicyclo[5.4.0]undec-7-ene; bis-triphenylphosphine-palladium(II) chloride; triphenylphosphine in N,N-dimethyl acetamide
参考文献
Perry, Robert J.; Wilson, B. David; Miller, Richard J.
Journal of Organic Chemistry, 1992 , vol. 57, # 10 p. 2883 - 2887
反应条件
triethylamine in diethyl ether 18 h; Ambient temperature;
参考文献
Perry, Robert J.; Wilson, B. David; Miller, Richard J.
Journal of Organic Chemistry, 1992 , vol. 57, # 10 p. 2883 - 2887
反应条件
in xylene 7 h; Heating;
参考文献
Hetzheim; Schlaak; Kerstan
Pharmazie, 1987 , vol. 42, # 2 p. 80 - 82
反应条件
1: lithium tert-butylate; iodine / tetrahydrofuran / 0.17 h / 20 °C 2: tetrahydrofuran / 1 h / 20 °C View Scheme
参考文献
Yotphan, Sirilata; Beukeaw, Danupat; Reutrakul, Vichai
Synthesis (Germany), 2013 , vol. 45, # 7 art. no. SS-2013-F0068-OP, p. 936 - 942
反应条件
in water T=60°C; 5 h;
参考文献
Sycheva,T.P. et al.
Chemistry of Heterocyclic Compounds (New York, NY, United States), 1966 , vol. 2, p. 144 - 148
Khimiya Geterotsiklicheskikh Soedinenii, 1966 , vol. 2, p. 205 - 211
反应条件
in tetrahydrofuran T=20°C; 1 h;
参考文献
Yotphan, Sirilata; Beukeaw, Danupat; Reutrakul, Vichai
Synthesis (Germany), 2013 , vol. 45, # 7 art. no. SS-2013-F0068-OP, p. 936 - 942
