1: 1,2-dibromo-3-chlorobenzene With isopropylmagnesium chloride in tetrahydrofuran T=-40°C; 2 h; 2: carbon dioxide With hydrogenchloride in tetrahydrofuran 1 h; Further stages.;
参考文献
Menzel, Karsten; Dimichele, Lisa; Mills, Paul; Frantz, Doug E.; Nelson, Todd D.; Kress, Michael H.
Synlett, 2006 , # 12 p. 1948 - 1952
1: With isopropylmagnesium chloride lithium chloride complex in tetrahydrofuran T=-40°C; 2: With hydrogenchloride in tetrahydrofuran Further stages. Title compound not separated from byproducts.;
1: 1,2-dibromo-3-chlorobenzene With isopropylmagnesium chloride in tetrahydrofuran T=-40°C; 2 h; 2: carbon dioxide With hydrogenchloride in tetrahydrofuran 1 h; Further stages.;
参考文献
Menzel, Karsten; Dimichele, Lisa; Mills, Paul; Frantz, Doug E.; Nelson, Todd D.; Kress, Michael H.
Synlett, 2006 , # 12 p. 1948 - 1952
1: With isopropylmagnesium chloride lithium chloride complex in tetrahydrofuran T=-40°C; 2: With hydrogenchloride in tetrahydrofuran Further stages. Title compound not separated from byproducts.;
