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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
104516-09-8
合成路线
（共 16 条）
104516-09-8
→
反应条件
1896-62-4
苄叉丙酮
反应条件
bis(trimethylsilyl)-peroxide; MoVIO2(acetylacetone)2 in dichloromethane T=25°C; 4 h;
参考文献
Matsubara; Okazoe; Oshima; Takai; Nozaki
Bulletin of the Chemical Society of Japan, 1985 , vol. 58, # 3 p. 844 - 849
104516-09-8
+
27607-77-8
三氟甲磺酸三甲基硅酯
→
反应条件
1427778-03-7
+
1896-62-4
苄叉丙酮
反应条件
in dichloromethane T=-78 - 25°C; 0.5 h; Inert atmosphere; stereoselective reaction;
参考文献
Sabbasani, Venkata R.; Mamidipalli, Phani; Lu, Huijie; Xia, Yuanzhi; Lee, Daesung
Organic Letters, 2013 , vol. 15, # 7 p. 1552 - 1555
104516-09-8
→
反应条件
5732-13-8
反应条件
C44H29O4P in dichloromethane T=20°C; 4 h; Inert atmosphere; optical yield given as percent eeenantioselective reaction;
参考文献
Wang, Yan; Zheng, Kuan; Hong, Ran
Journal of the American Chemical Society, 2012 , vol. 134, # 9 p. 4096 - 4099
104516-09-8
→
反应条件
17113-33-6
2-苯基呋喃
反应条件
1: DMP / CH2Cl2 / Ambient temperature 2: 5 percent / TCPCTFE / acetone View Scheme
参考文献
Journal of Organic Chemistry, , vol. 62, # 21 p. 7295 - 7304
104516-09-8
→
反应条件
16939-57-4
反式-1-苯基-1,3-丁二烯
反应条件
1: 62 percent / LiBr; acetic acid / palladium(II) acetate / 1 h / 40 °C 2: 56 percent / triethylamine; pinacolborane; DPEphos / palladium(II) acetate / dioxane; tetrahydrofuran / 5 h / 100 °C View Scheme
参考文献
Tetrahedron, , vol. 63, # 45 p. 10939 - 10948
104516-09-8
+
688-73-3
三正丁基氢化锡
→
反应条件
反应条件
Mo(CO)3(CN-t-Bu)3; hydroquinone in tetrahydrofuran T=55°C; 10 h;
参考文献
Journal of Organic Chemistry, , vol. 71, # 6 p. 2429 - 2433
104516-09-8
→
反应条件
124244-39-9
+
175274-01-8
反应条件
AgOTf; 2,6-bis[(4S)-isopropyl-2-oxazolin-2-yl]pyridine in dichloromethane T=-10°C; 22 h; Inert atmosphere; optical yield given as percent eeenantioselective reaction;
参考文献
Wang, Yan; Zheng, Kuan; Hong, Ran
Journal of the American Chemical Society, 2012 , vol. 134, # 9 p. 4096 - 4099
104516-09-8
→
反应条件
5732-13-8
+
124244-39-9
+
175274-01-8
反应条件
Ag(1+)*C44H28O4P(1-) in dichloromethane T=20°C; 4 h; Inert atmosphere; optical yield given as percent eeenantioselective reaction;
参考文献
Wang, Yan; Zheng, Kuan; Hong, Ran
Journal of the American Chemical Society, 2012 , vol. 134, # 9 p. 4096 - 4099
104516-09-8
→
反应条件
5732-13-8
+
124244-39-9
+
175274-01-8
反应条件
Ag(1+)*C44H28O4P(1-) in dichloromethane T=-10°C; 48 h; Inert atmosphere; optical yield given as percent eeenantioselective reaction;
参考文献
Wang, Yan; Zheng, Kuan; Hong, Ran
Journal of the American Chemical Society, 2012 , vol. 134, # 9 p. 4096 - 4099
104516-09-8
→
反应条件
124244-39-9
+
175274-01-8
反应条件
AgOTf; 2,6-bis[(4S)-isopropyl-2-oxazolin-2-yl]pyridine in dichloromethane T=-10°C; 22 h; Inert atmosphere; optical yield given as percent eeenantioselective reaction;
参考文献
Wang, Yan; Zheng, Kuan; Hong, Ran
Journal of the American Chemical Society, 2012 , vol. 134, # 9 p. 4096 - 4099
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