2,4-二(三甲硅氧基)嘧啶合成路线 （共 49 条）
反应条件
ammonium sulfate 2 h; RefluxLarge scale;
参考文献
Organic Process Research and Development, , vol. 8, # 4 p. 564 - 567
反应条件
ammonium sulfate 4 h; Heating;
参考文献
Nucleosides and Nucleotides, , vol. 15, # 1-3 p. 183 - 204
反应条件
in acetonitrile 0.5 h; Ambient temperature;
参考文献
Journal of the Chemical Society. Perkin Transactions 2, , # 11 p. 2343 - 2349
参考文献
US2004/204420 A1, ;
Page/Page column Figure 9 ;
反应条件
3 h; Ambient temperature;
参考文献
Phytochemistry, , vol. 50, # 2 p. 337 - 338
反应条件
trimethylsilyl trifluoromethanesulfonate; mercury(II) diacetate; hydroquinone 4 h; Heating;
参考文献
Dalpozzo, Renato; De Nino, Antonio; Maiuolo, Loredana; Procopio, Antonio; Romeo, Roberto; Sindona, Giovanni
Synthesis, 2002 , # 2 p. 172 - 174
反应条件
tin(IV) chloride in 1,2-dichloro-ethane T=20 - 83°C; 22 h; Product distribution / selectivity;
参考文献
SICOR INC.
Patent: WO2006/63105 A1, 2006 ;
Location in patent: Page/Page column 11-12 ;
反应条件
trimethylsilyl trifluoromethanesulfonate in 1,2-dichloro-ethane T=83°C; 17 h; Product distribution / selectivity;
参考文献
Chou; Heath; Patterson; Poteet; Lakin; Hunt
Synthesis, 1992 , # 6 p. 565 - 570
反应条件
O-(2,4,6-trimethylbenzenesulfonyl)hydroxylamine in dichloromethane 3 h; Ambient temperature;
参考文献
Imaizumi; Kano; Sakata
Chemical and Pharmaceutical Bulletin, 1992 , vol. 40, # 7 p. 1808 - 1813
反应条件
tin(IV) chloride in 1,2-dichloro-ethane T=20 - 83°C; 22 h; Product distribution / selectivity;
参考文献
SICOR INC.
Patent: WO2006/63105 A1, 2006 ;
Location in patent: Page/Page column 11-12 ;
