2,4-二(三甲硅氧基)嘧啶合成路线 （共 49 条）
反应条件
silver trifluoromethanesulfonate; diphenyltin sulfide in 1,2-dichloro-ethane; acetonitrile T=60°C; 6 h;
参考文献
Mukaiyama, Teruaki; Matsutani, Takafumi; Shimomura, Naoyuki
Chemistry Letters, 1993 , # 9 p. 1627 - 1630
反应条件
stannous iodide in acetonitrile T=60°C; 6 h;
参考文献
Mukaiyama, Teruaki; Nagai, Masashi; Matsutani, Takafumi; Shimomura, Naoyuki
Nucleosides and Nucleotides, 1996 , vol. 15, # 1-3 p. 17 - 30
反应条件
2,6-di-tert-butyl-4-methylpyridinium triflate in acetonitrile T=100°C; silyl-Hilbert-Johnson reaction; 0.333333 h; tubing reactor;
参考文献
Angewandte Chemie - International Edition, , vol. 50, # 9 p. 2155 - 2158
反应条件
silver trifluoromethanesulfonate; diphenyltin sulfide in acetonitrile T=60°C; 4 h;
参考文献
Shimomura; Matsutani; Mukaiyama
Bulletin of the Chemical Society of Japan, 1994 , vol. 67, # 11 p. 3100 - 3106
反应条件
tin(IV) chloride in chloroform T=20°C; Vorbruggen glycosylation; 5 h;
参考文献
Nucleosides, Nucleotides and Nucleic Acids, , vol. 23, # 4 p. 655 - 669
反应条件
silicon tetrafluoride in acetonitrile T=0°C; 2 h;
参考文献
Noyori, Ryoji; Hayashi, Masahiko
Chemistry Letters, 1987 , p. 57 - 60
反应条件
ammonium sulfate; N,O-bis-(trimethylsilyl)-acetamide in acetonitrile T=80°C; 3.5 h; Reflux;
参考文献
Lazrek, Hassan B.; Ouzebla, Driss; Faraj, Abdesslem
Nucleosides, Nucleotides and Nucleic Acids, 2011 , vol. 30, # 3 p. 227 - 234
反应条件
pyridine; tin(IV) chloride 1) acetonitrile, room temp., 2 days; 2) chloroform, 30 min., reflux; Yield given. Multistep reaction;
参考文献
Holy, Antonin; Koenig, Joachim; Vesely, Jiri; Cech, Dieter; Votruba, Ivan; Clercq, Erik de
Collection of Czechoslovak Chemical Communications, 1987 , vol. 52, # 6 p. 1589 - 1608
反应条件
trimethylsilyl trifluoromethanesulfonate in 1,2-dichloro-ethane
T=20°C; 16 h;
参考文献
Mikhailov, Sergei N.; Padyukova, Nelly Sh.; Karpeiskii, Marat Ya.; Kolobushkina, Lidiya I.; Beigelman, Leon N.
Collection of Czechoslovak Chemical Communications, 1989 , vol. 54, # 4 p. 1055 - 1066
反应条件
iodine in 1,2-dichloro-ethane
36 h; Heating;
参考文献
Malik, Vaishali; Singh, Palwinder; Kumar, Subodh
Tetrahedron, 2005 , vol. 61, # 16 p. 4009 - 4014
