N4-苯甲酰基-2'-脱氧-5-甲基胞苷合成路线 （共 6 条）
反应条件
in pyridine 1.) 0 deg C, 10 min; 2.) r.t., 3 h;
参考文献
Uesugi; Miyashiro; Tomita; Ikehara
Chemical and Pharmaceutical Bulletin, 1986 , vol. 34, # 1 p. 51 - 60
反应条件
1: POCl3; triazole / pyridine / 4 h / 20 °C 2: NH3 / 0.33 h / 0 °C 3: pyridine / 16 h / 20 °C 4: NaOH / H2O / 0.08 h / 0 °C View Scheme
参考文献
Busson; Kerremans; Van Aerschot; Peeters; Blaton; Herdewijn
Nucleosides and Nucleotides, 1999 , vol. 18, # 4-5 p. 1079 - 1082
反应条件
1: pyridine / 16 h / 20 °C 2: NaOH / H2O / 0.08 h / 0 °C View Scheme
参考文献
Busson; Kerremans; Van Aerschot; Peeters; Blaton; Herdewijn
Nucleosides and Nucleotides, 1999 , vol. 18, # 4-5 p. 1079 - 1082
反应条件
1: NH3 / 0.33 h / 0 °C 2: pyridine / 16 h / 20 °C 3: NaOH / H2O / 0.08 h / 0 °C View Scheme
参考文献
Busson; Kerremans; Van Aerschot; Peeters; Blaton; Herdewijn
Nucleosides and Nucleotides, 1999 , vol. 18, # 4-5 p. 1079 - 1082
反应条件
1: pyridine / 16 h / 20 °C 2: POCl3; triazole / pyridine / 4 h / 20 °C 3: NH3 / 0.33 h / 0 °C 4: pyridine / 16 h / 20 °C 5: NaOH / H2O / 0.08 h / 0 °C View Scheme
参考文献
Busson; Kerremans; Van Aerschot; Peeters; Blaton; Herdewijn
Nucleosides and Nucleotides, 1999 , vol. 18, # 4-5 p. 1079 - 1082
反应条件
in pyridine
2 h; Ambient temperature;
参考文献
Uesugi; Miyashiro; Tomita; Ikehara
Chemical and Pharmaceutical Bulletin, 1986 , vol. 34, # 1 p. 51 - 60
