5-甲基-2-异丙基环己酮合成路线 (共 238 条)
反应条件
titanium tetrachloride; magnesium; tert-butyl alcohol in tetrahydrofuran 48 h; Ambient temperature; Yield given. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Tetrahedron Letters, , vol. 27, # 35 p. 4153 - 4156
反应条件
hydrogenchloride in benzene Yields of byproduct given;
参考文献
Menon; Kumar; Ravindranathan
Tetrahedron Letters, 1987 , vol. 28, # 44 p. 5313 - 5314
反应条件
in tetrahydrofuran T=-78°C; Methylation; 1 h;
参考文献
Heterocycles, , vol. 52, # 3 p. 1029 - 1032
反应条件
3-chloro-benzenecarboperoxoic acid in chloroform 20 h; Heating; Further byproducts given;
参考文献
Phytochemistry (Elsevier), , vol. 27, # 12 p. 3861 - 3870
反应条件
HOF* CH3CN; NAF in chloroform; water; acetonitrile 0 deg C -> room temperature;
参考文献
Journal of Organic Chemistry, , vol. 60, # 25 p. 8267 - 8269
反应条件
n-butyllithium; (1R,3S,5R)-1,3,5-trimethyl-5-lt;(4S,5S)-4,5-diphenyl-Δ2-oxazolin-2-ylgt;cyclohexane-1,3-dicarboxylic acid imide in tetrahydrofuran T=-78°C; 2 h; Yield given. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Synlett, , # SPEC. ISS. p. 411 - 420
反应条件
N,N,N',N',N'',N''-hexamethylphosphoric triamide in tetrahydrofuran T=-105°C; 0.833333 h; Yield given. Further byproducts given;
参考文献
Tetrahedron Letters, , vol. 30, # 47 p. 6537 - 6540
反应条件
in chloroform 24 h; Ambient temperature;
参考文献
Doleschall, Gabor; Toth, Gabor
Tetrahedron, 1980 , vol. 36, p. 1649 - 1666
反应条件
silica gel; ozone T=-60 - -50°C; 3 h;
参考文献
Phytochemistry (Elsevier), , vol. 27, # 12 p. 3861 - 3870
反应条件
3-chloro-benzenecarboperoxoic acid in chloroform 20 h; Heating; Further byproducts given;
参考文献
Phytochemistry (Elsevier), , vol. 27, # 12 p. 3861 - 3870