lead(IV) acetate; triethylamine in N,N-dimethyl-formamide T=80°C; 1 h;
参考文献
Francis, John E.; Cash, William D.; Barbaz, Beverly S.; Bernard, Patrick S.; Lovell, Richard A.; et al.
Journal of Medicinal Chemistry, 1991 , vol. 34, # 1 p. 281 - 290
Multi-step reaction with 3 steps 1: 1.) 10 N NaOH / 1.) THF, 80 deg C, 15 min, 2.) 2-methoxyethanol, reflux2: 83 percent / NaOMe / ethanol3: 92 percent / 85percent aq. H2SO4 / 1.5 h / 80 °C
参考文献
Francis, John E.; Cash, William D.; Barbaz, Beverly S.; Bernard, Patrick S.; Lovell, Richard A.; et al. Journal of Medicinal Chemistry, 1991 , vol. 34, # 1 p. 281 - 290
Multi-step reaction with 3 steps 1: 1.) 10 N NaOH / 1.) THF, 80 deg C, 15 min, 2.) 2-methoxyethanol, reflux2: 83 percent / NaOMe / ethanol3: 92 percent / 85percent aq. H2SO4 / 1.5 h / 80 °C
参考文献
Francis, John E.; Cash, William D.; Barbaz, Beverly S.; Bernard, Patrick S.; Lovell, Richard A.; et al. Journal of Medicinal Chemistry, 1991 , vol. 34, # 1 p. 281 - 290
