1: 85 percent / DMDO / acetone / 1 h / 20 °C 2: 84 percent / aq. HClO4 / 0.17 h / 0 °C 3: 52 percent / NaBH3CN; glacial acetic acid 4: 82 percent / (COCl)2; DMF / CH2Cl2 / 0.5 h 5: NaN3 / tetrahydrofuran / 4 h View Scheme
参考文献
Larsen, David S.; Lins, Roger J.; Stoodley, Richard J.; Trotter, Nicholas S.
Journal of the Chemical Society. Perkin Transactions 1, 2001 , # 18 p. 2204 - 2212
1: 85 percent / DMDO / acetone / 1 h / 20 °C 2: 84 percent / aq. HClO4 / 0.17 h / 0 °C 3: 52 percent / NaBH3CN; glacial acetic acid 4: 82 percent / (COCl)2; DMF / CH2Cl2 / 0.5 h 5: NaN3 / tetrahydrofuran / 4 h View Scheme
参考文献
Larsen, David S.; Lins, Roger J.; Stoodley, Richard J.; Trotter, Nicholas S.
Journal of the Chemical Society. Perkin Transactions 1, 2001 , # 18 p. 2204 - 2212
1: 85 percent / DMDO / acetone / 1 h / 20 °C 2: 84 percent / aq. HClO4 / 0.17 h / 0 °C 3: 52 percent / NaBH3CN; glacial acetic acid 4: 82 percent / (COCl)2; DMF / CH2Cl2 / 0.5 h 5: NaN3 / tetrahydrofuran / 4 h View Scheme
参考文献
Larsen, David S.; Lins, Roger J.; Stoodley, Richard J.; Trotter, Nicholas S.
Journal of the Chemical Society. Perkin Transactions 1, 2001 , # 18 p. 2204 - 2212
