5-苄基-5,11-二氢-10H-二苯并[b,f]氮杂卓-10-酮合成路线 （共 7 条）
反应条件
n-butyllithium; N,N,N',N,-tetramethylethylenediamine; lithium diisopropyl amide in tetrahydrofuran; hexane T=-20°C; 4 h;
参考文献
Lohse, Olivier; Beutler, Ulrich; Fuenfschilling, Peter; Furet, Pascal; France, Julien; Kaufmann, Daniel; Penn, Gerhard; Zaugg, Werner
Tetrahedron Letters, 2001 , vol. 42, # 3 p. 385 - 389
反应条件
1: 88 percent / NaOtBu / Pd(OAc)2; rac-BINAP / toluene 2: 97 percent / NaH / dimethylformamide 3: 86 percent / LDA; TMEDA; n-BuLi / tetrahydrofuran; hexane / 4 h / -20 °C View Scheme
参考文献
Tetrahedron Letters, , vol. 42, # 3 p. 385 - 389
反应条件
1: 88 percent / NaOtBu / Pd(OAc)2; rac-BINAP / toluene 2: 97 percent / NaH / dimethylformamide 3: 86 percent / LDA; TMEDA; n-BuLi / tetrahydrofuran; hexane / 4 h / -20 °C View Scheme
参考文献
Tetrahedron Letters, , vol. 42, # 3 p. 385 - 389
反应条件
1: 97 percent / NaH / dimethylformamide 2: 86 percent / LDA; TMEDA; n-BuLi / tetrahydrofuran; hexane / 4 h / -20 °C View Scheme
参考文献
Tetrahedron Letters, , vol. 42, # 3 p. 385 - 389
反应条件
1: 97 percent / NaH / dimethylformamide 2: 86 percent / LDA; TMEDA; n-BuLi / tetrahydrofuran; hexane / 4 h / -20 °C View Scheme
参考文献
Tetrahedron Letters, , vol. 42, # 3 p. 385 - 389
反应条件
1: 75 percent / TMSCl; NaI / acetonitrile 2: 80 percent View Scheme
参考文献
Lohse, Olivier; Beutler, Ulrich; Fuenfschilling, Peter; Furet, Pascal; France, Julien; Kaufmann, Daniel; Penn, Gerhard; Zaugg, Werner
Tetrahedron Letters, 2001 , vol. 42, # 3 p. 385 - 389
反应条件
chloro-trimethyl-silane; sodium iodide in acetonitrile
参考文献
Lohse, Olivier; Beutler, Ulrich; Fuenfschilling, Peter; Furet, Pascal; France, Julien; Kaufmann, Daniel; Penn, Gerhard; Zaugg, Werner
Tetrahedron Letters, 2001 , vol. 42, # 3 p. 385 - 389
