N-(3-氨基-1H-1,2,4-三唑-5-基)苯磺酰胺合成路线 （共 6 条）
反应条件
potassium hydroxide in ethylene glycol T=170°C; 1.5 h;
参考文献
Maybhate; Rajamohanan; Rajappa
Synthesis, 1991 , # 3 p. 220 - 222
反应条件
hydrazine in acetonitrile 48 h; Ambient temperature;
参考文献
Kleschick, William A.; Dunbar, Joseph E.; Snider, Sigrid W.; Vinogradoff, Anna P.
Journal of Organic Chemistry, 1988 , vol. 53, # 13 p. 3120 - 3122
反应条件
1.1: K2CO3 / dimethylformamide / 15 h / 20 °C 1.2: 82 percent / aq. HCl / dimethylformamide / 8 h / 20 °C 2.1: acetonitrile / 16 h / 60 °C 3.1: SO2Cl2 / CH2Cl2 / 20 °C 4.1: aq. ethanol / 0.25 h / Heating View Scheme
参考文献
Kleschick, William A.; Dunbar, Joseph E.; Snider, Sigrid W.; Vinogradoff, Anna P.
Journal of Organic Chemistry, 1988 , vol. 53, # 13 p. 3120 - 3122
反应条件
1: SO2Cl2 / CH2Cl2 / 20 °C 2: aq. ethanol / 0.25 h / Heating View Scheme
参考文献
Chibale, Kelly; Dauvergne, Jerome; Wyatt, Paul G.
Synthesis, 2002 , # 2 p. 185 - 190
反应条件
1: With pyridine 0.05 h; Reflux; 2: With water; sodium hydroxide Reflux; regioselective reaction;
参考文献
Chernyshov; Kozlenko; Taranushich
Russian Journal of Applied Chemistry, 2011 , vol. 84, # 2 p. 230 - 235
反应条件
trifluoroacetic acid
参考文献
Chibale, Kelly; Dauvergne, Jerome; Wyatt, Paul G.
Synthesis, 2002 , # 2 p. 185 - 190
