2-(3,4-二氢-2H-吡喃-5-基)-4,4,5,5-四甲基-1,3,2-二噁硼烷合成路线 （共 3 条）
反应条件
potassium acetate; dichloro(1,1'-bis(diphenylphosphanyl)ferrocene)palladium(II) dichloromethane adduct in 1,4-dioxane T=80°C; 12 h; Inert atmosphere;
参考文献
WO2010/57121 A1, ;
Page/Page column 142 ;
WO 2010/057121 A1
反应条件
4,4'-di-tert-butyl-2,2'-dipyridyl; bis(η4-1,5-cyclooctadiene)-di-μ-methoxy-diiridium(I) in octane T=80°C; 8 h; Title compound not separated from byproducts.;
参考文献
Chemistry Letters, , vol. 37, # 6 p. 664 - 665
反应条件
catalyst:(Ir(COD)OCH3)2/2(4,4'-di-tert-butyl-bipy) in hexane heating in hexane at 25-80°C in the presence of (Ir(OMe)(COD))2/2(4,4'-di-tert-butyl-bipy); (.alpha/β=95/5);
参考文献
Bulletin of the Chemical Society of Japan, , vol. 81, # 12 p. 1535 - 1553
