4’-甲基-2,2’-联吡啶-4-甲醛合成路线 （共 9 条）
反应条件
selenium(IV) oxide in 1,4-dioxane 24 h; Heating;
参考文献
Khairoutdinov, Rafail F.; Doubova, Larissa V.; Haddon, Robert C.; Saraf, Laxmikant
Journal of Physical Chemistry B, 2004 , vol. 108, # 52 p. 19976 - 19981
反应条件
selenium(IV) oxide in 1,4-dioxane 72 h;
参考文献
Eckermann, Amanda L.; Barker, Kylie D.; Hartings, Matthew R.; Ratner, Mark A.; Meade, Thomas J.
Journal of the American Chemical Society, 2005 , vol. 127, # 34 p. 11880 - 11881
反应条件
manganese(IV) oxide in dichloromethane Ambient temperatureovernight;
参考文献
Ciana, Leopoldo Della; Hamachi, Itaru; Meyer, Thomas J.
Journal of Organic Chemistry, 1989 , vol. 54, # 7 p. 1731 - 1735
反应条件
1: 59 percent / Pd/C 2: 50 percent / SeO2 / dioxane / 24 h / Heating View Scheme
参考文献
Chin, Teen; Gao, Zhinong; Lelouche, Isabelle; Shin, Yeung-Gyo K.; Purandare, Ashok; Knapp, Spencer; Isied, Stephan S.
Journal of the American Chemical Society, 1997 , vol. 119, # 52 p. 12849 - 12858
反应条件
1: 1.) acetic anhydride, 2.) 10percent aq. NaOH / 1.) 60-65 deg C, 24 h, 2.) aq. EtOH, reflux, 30 min 2: 58 percent / MnO2 / CH2Cl2 / Ambient temperature; overnight View Scheme
参考文献
Ciana, Leopoldo Della; Hamachi, Itaru; Meyer, Thomas J.
Journal of Organic Chemistry, 1989 , vol. 54, # 7 p. 1731 - 1735
反应条件
sodium tetrahydroborate in ethanol 1.5 h; Ambient temperature;
参考文献
Furue, Masaoki; Yoshidzumi, Toshiyuki; Kinoshita, Shuichi; Kushida, Takashi; Nozakura, Shun-ichi; Kamachi, Mikiharu
Bulletin of the Chemical Society of Japan, 1991 , vol. 64, # 5 p. 1632 - 1640
反应条件
1: 1.2 g / NaBH4; aq. NaOH / methanol / 1 h / 20 °C 2: 98 percent / aq. HBr; H2SO4 / Heating View Scheme
参考文献
Furue, Masaoki; Yoshidzumi, Toshiyuki; Kinoshita, Shuichi; Kushida, Takashi; Nozakura, Shun-ichi; Kamachi, Mikiharu
Bulletin of the Chemical Society of Japan, 1991 , vol. 64, # 5 p. 1632 - 1640
反应条件
sodium hydroxide; silver nitrate in ethanol; water 24 h;
参考文献
Aldridge III, W. Steven; Hornstein, Brooks J.; Serron, Scafford; Dattelbaum, Dana M.; Schoonover, Jon R.; Meyer, Thomas J.
Journal of Organic Chemistry, 2006 , vol. 71, # 14 p. 5186 - 5190
反应条件
1: NaBH4
2: SO2Br / CH2Cl2
3: Ambient temperature
View Scheme
参考文献
Furue, Masaoki; Yoshidzumi, Toshiyuki; Kinoshita, Shuichi; Kushida, Takashi; Nozakura, Shun-ichi; Kamachi, Mikiharu
Bulletin of the Chemical Society of Japan, 1991 , vol. 64, # 5 p. 1632 - 1640
