2,3-二甲基-3-丁烯-2-醇合成路线 （共 74 条）
参考文献
Ogloblin
Zhurnal Obshchei Khimii, 1948 , vol. 18, p. 2157
Chem.Abstr., 1949 , p. 3777
反应条件
1: in diethyl ether
T=-78 - 20°C; 17.25 h; Inert atmosphere;
2: With ammonium chloride in diethyl ether; water
T=0°C;
参考文献
Takahashi, Masayuki; McLaughlin, Martin; Micalizio, Glenn C.
Angewandte Chemie, International Edition, 2009 , vol. 48, # 20 p. 3648 - 3652
反应条件
sodium tetrahydroborate in methanol
T=25°C; 2 h; Title compound not separated from byproducts.;
参考文献
Singleton, Daniel A.; Hang, Chao; Szymanski, Michael J.; Meyer, Matthew P.; Leach, Andrew G.; Kuwata, Keith T.; Chen, Jenny S.; Greer, Alexander; Foote, Christopher S.; Houk
Journal of the American Chemical Society, 2003 , vol. 125, # 5 p. 1319 - 1328
参考文献
Chupotsky; Marioza
Zhurnal Russkago Fiziko-Khimicheskago Obshchestva, 1889 , vol. 21, p. 432
反应条件
sulfuric acid in dichloromethane-d2
T=26.5°C; acid conc. below 10 mmol/l;
参考文献
Zon, A. van; Huis, R.
Recueil: Journal of the Royal Netherlands Chemical Society, 1981 , vol. 100, # 11 p. 425 - 429
反应条件
in diethyl ether
16 h; Heating;
参考文献
Kraft, Philip; Popaj, Kasim
European Journal of Organic Chemistry, 2004 , # 24 p. 4995 - 5002
反应条件
oxygen; bis(.eta.(2)-ethylene)(2,4,-pentanedionato)rhodium in toluene
T=80°C; P=37503 Torr; 1 h;
参考文献
Boennemann, Helmut; Nunez, Washington; Rohe, Dieter M. M.
Helvetica Chimica Acta, 1983 , vol. 66, # 1 p. 177 - 185
反应条件
diethyl ether; triphenylphosphine
参考文献
Schenck; Schulte-Elte
Justus Liebigs Annalen der Chemie, 1958 , vol. 618, p. 185,191
反应条件
perchloric acid; sodium perchlorate
T=25°C; Yields of byproduct given;
参考文献
Pocker, Y.; Ronald, B. P.
Journal of the American Chemical Society, 1980 , vol. 102, # 16 p. 5311 - 5316
反应条件
in toluene
T=100°C; 24 h;
参考文献
Robinson, Philip L.; Barry, Carey N.; Kelly, Jeffery W.; Evans, Slayton A.
Journal of the American Chemical Society, 1985 , vol. 107, # 18 p. 5210 - 5219
