3-甲基-3-丁烯-2-醇合成路线 （共 65 条）
反应条件
1: LiAlH4 / diethyl ether / 4 h / Heating
2: 62.1 percent Chromat. / NaNO2, HClO4
View Scheme
参考文献
Kirmse, Wolfgang; Rode, Jutta; Rode, Klaus
Chemische Berichte, 1986 , vol. 119, # 12 p. 3672 - 3693
反应条件
water; calcium carbonate
T=70°C; (+-)-methylisopropenylcarbinol;
参考文献
Tischtschenko
Zhurnal Obshchei Khimii, 1936 , vol. 6, p. 1551
Chem. Zentralbl., 1937 , vol. 108, # I p. 3785
反应条件
perchloric acid; sodium nitrite
参考文献
Kirmse, Wolfgang; Rode, Jutta; Rode, Klaus
Chemische Berichte, 1986 , vol. 119, # 12 p. 3672 - 3693
参考文献
Cox,E.F. et al.
Journal of the American Chemical Society, 1961 , vol. 83, p. 2719 - 2724
反应条件
1: LiAlH4 / diethyl ether / Heating
2: 62.1 percent Chromat. / NaNO2, HClO4
View Scheme
参考文献
Kirmse, Wolfgang; Rode, Jutta; Rode, Klaus
Chemische Berichte, 1986 , vol. 119, # 12 p. 3672 - 3693
反应条件
1: 1.) (C2H5)3N, ClCOOEt, 2.) NH3 / 1.) toluene, 0 deg C, 2 h, 2.) toluene, ca. 1 h
2: LiAlH4 / diethyl ether / Heating
3: 62.1 percent Chromat. / NaNO2, HClO4
View Scheme
参考文献
Kirmse, Wolfgang; Rode, Jutta; Rode, Klaus
Chemische Berichte, 1986 , vol. 119, # 12 p. 3672 - 3693
参考文献
Chen, Yu-Zhe; Wu, Li-Zhu; Zhang, Li-Ping; Tung, Chen-Ho
Journal of Organic Chemistry, 2005 , vol. 70, # 12 p. 4676 - 4681
反应条件
C32H28N4O4; oxygen in acetonitrile
2 h; UV-irradiation;
参考文献
Geer, Michael F.; Walla, Michael D.; Solntsev, Kyril M.; Strassert, Cristian A.; Shimizu, Linda S.
Journal of Organic Chemistry, 2013 , vol. 78, # 11 p. 5568 - 5578
反应条件
water; chlorine
man schuettelt die waessr.Schicht mit K2CO3 und hebt den gebildeten Alkohol ab;
参考文献
Kondakow
Zhurnal Russkago Fiziko-Khimicheskago Obshchestva, 1885 , vol. 17, p. 296
Chemische Berichte, 18 Ref. <1885>,661
反应条件
sodium carbonate
(+-)-methylisopropenylcarbinol;
参考文献
Gutner; Tischtschenko
Zhurnal Obshchei Khimii, 1938 , vol. 8, p. 1066
Chem. Zentralbl., 1939 , vol. 110, # II p. 4221
