3-甲基-3-丁烯-2-醇合成路线 （共 65 条）
反应条件
1: NaHCO3; chlorine / -10 - -8 °C
2: Na2CO3
View Scheme
参考文献
Gutner; Tischtschenko
Zhurnal Obshchei Khimii, 1938 , vol. 8, p. 1066
Chem. Zentralbl., 1939 , vol. 110, # II p. 4221
反应条件
magnesium
1.) ether, 10 deg C; 2.) -10 deg C; Multistep reaction;
参考文献
Georgoulis, Constantin; Smadja, William; Ville, Guy
Bulletin de la Societe Chimique de France, 1984 , vol. 2, # 7-8 p. 269 - 270
反应条件
perchloric acid; sodium nitrite
参考文献
Kirmse, Wolfgang; Rode, Jutta; Rode, Klaus
Chemische Berichte, 1986 , vol. 119, # 12 p. 3672 - 3693
反应条件
magnesium bromide in N,N-dimethyl-formamide
T=130°C; Isomerization; KineticsProduct distribution; Further Variations:ReagentsSolventsTemperatures;
参考文献
Shemanaeva; Mel'nik; Razina; Egorova; Kryukov
Petroleum Chemistry, 1999 , vol. 39, # 3 p. 191 - 195
参考文献
Tischtschenko
Zhurnal Obshchei Khimii, 1936 , vol. 6, p. 1551
Chem. Zentralbl., 1937 , vol. 108, # I p. 3785
参考文献
Tischtschenko
Zhurnal Obshchei Khimii, 1936 , vol. 6, p. 1551
Chem. Zentralbl., 1937 , vol. 108, # I p. 3785
反应条件
1: 98 percent / propionic acid / 1 h / 180 °C
2: 92 percent / LiAlH4 / diethyl ether / 2 h / Ambient temperature
3: 51 percent / 1.) pyridinium chlorochromate / CH2Cl2 / 1.) 0 deg C, 2.) reflux
View Scheme
参考文献
Ho, Nan-hui; Noble, W. J. le
Journal of Organic Chemistry, 1989 , vol. 54, # 8 p. 2018 - 2021
反应条件
1,4-di(diphenylphosphino)-butane; bis(dibenzylideneacetone)-palladium(0) in ethylene glycol dimethyl ether
T=190°C; P=30400 Torr; 48 h;
参考文献
El Ali, Bassam; Alper, Howard
Journal of Organic Chemistry, 1991 , vol. 56, # 18 p. 5357 - 5360
参考文献
Crout, David H.G.; Morrey, Stephen M.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1983 , # 10 p. 2435 - 2440
反应条件
1: 94 percent / pyridine / 5 h
2: diethyl ether / 0 °C
View Scheme
参考文献
Crout, David H.G.; Morrey, Stephen M.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1983 , # 10 p. 2435 - 2440
