3beta-乙酰氧基-5-氧代-5,6-开链胆烷-6-酸合成路线 (共 6 条)
反应条件
ozone in pentane T=-60°C; Oxidation; ring cleavage; 0.666667 h;
参考文献
Xie; Peng; Zalkow; Li; Zhu; Powis; Kunkel
Bioorganic and medicinal chemistry, 2000 , vol. 8, # 4 p. 699 - 706
反应条件
jones reagent in acetone T=50°C;
参考文献
Epifanio, Rosangela de A.; Camargo, Wilson; Pinto, Angelo C.
Tetrahedron Letters, 1988 , vol. 29, # 49 p. 6403 - 6406
反应条件
chromium(VI) oxide; acetic acid
参考文献
Dauben; Fonken
Journal of the American Chemical Society, 1956 , vol. 78, p. 4736,4741
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Sorm
Collection of Czechoslovak Chemical Communications, 1947 , vol. 12, p. 436,439
反应条件
meta-chloroperoxybenzoic acid in chloroform
参考文献
Knof,L.
Justus Liebigs Annalen der Chemie, 1961 , vol. 647, p. 53 - 61
反应条件
1: 55 percent / m-chloroperbenzoic acid / benzene / 36 h / 20 °C 2: 5 mg / silica gel (70-230 mesh) / 20 h View Scheme
参考文献
Medelovici, Marioara; Glotter, Erwin
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1992 , # 13 p. 1735 - 1740
反应条件
tetraphosphorus decasulfide in pyridine
参考文献
Kasal
Collection of Czechoslovak Chemical Communications, 1983 , vol. 48, # 5 p. 1489 - 1498