3-(2-甲基苯基)丙酸乙酯合成路线 （共 17 条）
反应条件
1: copper diacetate; silver(I) acetate; [Cp*Ru(CH3CN)3][SbF6]2 / 1,1-dimethylpropan-1-ol / 24 h / 90 °C / |Schlenk technique; |Inert atmosphere; |Sealed tube 2: Raney-Nickel / ethanol / 1 h / 20 °C View Scheme
参考文献
Zhang, Xi-Sha; Zhu, Qi-Lei; Zhang, Yun-Fei; Li, Yan-Bang; Shi, Zhang-Jie
Chemistry - A European Journal, 2013 , vol. 19, # 36 p. 11898 - 11903
反应条件
1: copper diacetate; silver(I) acetate; [Cp*Ru(CH3CN)3][SbF6]2 / 1,1-dimethylpropan-1-ol / 24 h / 90 °C / |Schlenk technique; |Inert atmosphere; |Sealed tube 2: Raney-Nickel / ethanol / 1 h / 20 °C View Scheme
参考文献
Zhang, Xi-Sha; Zhu, Qi-Lei; Zhang, Yun-Fei; Li, Yan-Bang; Shi, Zhang-Jie
Chemistry - A European Journal, 2013 , vol. 19, # 36 p. 11898 - 11903
反应条件
1: copper diacetate; silver(I) acetate; [Cp*Ru(CH3CN)3][SbF6]2 / methanol / 24 h / 120 °C / |Schlenk technique; |Inert atmosphere; |Sealed tube 2: Raney-Nickel / ethanol / 1 h / 20 °C View Scheme
参考文献
Zhang, Xi-Sha; Zhu, Qi-Lei; Zhang, Yun-Fei; Li, Yan-Bang; Shi, Zhang-Jie
Chemistry - A European Journal, 2013 , vol. 19, # 36 p. 11898 - 11903
反应条件
zinc; benzene anschliessend Behandeln mit wss. Schwefelsaeure und Erhitzen des Reaktionsprodukts mit wenig Toluol-sulfonsaeure-(4);
参考文献
Grundmann
Chemische Berichte, 1948 , vol. 81, p. 512
参考文献
Harvey; Heilbron; Wilkinson
Journal of the Chemical Society, 1930 , p. 423,429
反应条件
1: diisobutylaluminum hydride / diethyl ether; toluene / -78 °C 2: oxalyl chloride; DMSO; Et3N / CH2Cl2 / -78 - 20 °C View Scheme
参考文献
Carroll, F. Ivy; Melvin, Matt S.; Nuckols, Michel C.; Mascarella, S. Wayne; Navarro, Hernan A.; Thomas, James B.
Journal of Medicinal Chemistry, 2006 , vol. 49, # 5 p. 1781 - 1791
反应条件
diisobutylaluminium hydride in diethyl ether; toluene
T=-78°C;
参考文献
Carroll, F. Ivy; Melvin, Matt S.; Nuckols, Michel C.; Mascarella, S. Wayne; Navarro, Hernan A.; Thomas, James B.
Journal of Medicinal Chemistry, 2006 , vol. 49, # 5 p. 1781 - 1791
