反应条件
1: N, N-dibenzylacetamide With 2,6-di-tert-butyl-4-methylpyridine; trifluoromethylsulfonic anhydride in dichloromethane
T=-78°C; 0.75 h;
2: ethylmagnesium bromide in diethyl ether; dichloromethane
T=-78 - 20°C; 1 h;
3: With lithium aluminium tetrahydride in diethyl ether; dichloromethane
T=20°C; 1 h;
参考文献
Xiao, Kai-Jiong; Wang, Yu; Ye, Ke-Yin; Huang, Pei-Qiang
Chemistry - A European Journal, 2010 , vol. 16, # 43 p. 12792 - 12796
