2-(2-甲基-1H-吡咯-1-基)乙醇合成路线 （共 7 条）
反应条件
potassium hydroxide in dimethyl sulfoxide T=20°C; Schlenk technique;
参考文献
Yang, Jin-Ming; Zhu, Cheng-Zhi; Tang, Xiang-Ying; Shi, Min
Angewandte Chemie - International Edition, 2014 , vol. 53, # 20 p. 5142 - 5146
Angew. Chem., 2014 , vol. 126, # 20 p. 5237 - 5241,5
反应条件
triethylamine in diethyl ether Reflux;
参考文献
Alberti, Mariza N.; Vougioukalakis, Georgios C.; Orfanopoulos, Michael
Journal of Organic Chemistry, 2009 , vol. 74, # 19 p. 7274 - 7282
反应条件
1: 1.) p-toluenesulfonic acid; 2.) p-toluenesulfonic acid, NaI/H2O / 1.) chloroform, 0 --> 20 deg C, 1 h; 2.) chloroform, reflux, 12 h 2: 92 percent / methanol / 48 h / 20 °C 3: 0.05N H2SO4 / H2O / 5 h / 50 °C 4: 74 percent / triethylamine / -15 deg C, 5h, then 50 deg C, 14 h View Scheme
参考文献
Cristau, Henri-Jean; Viala, Jacques; Christol, Henri
Bulletin de la Societe Chimique de France, 1985 , # 5 p. 980 - 998
反应条件
1: 92 percent / methanol / 48 h / 20 °C 2: 0.05N H2SO4 / H2O / 5 h / 50 °C 3: 74 percent / triethylamine / -15 deg C, 5h, then 50 deg C, 14 h View Scheme
参考文献
Cristau, Henri-Jean; Viala, Jacques; Christol, Henri
Bulletin de la Societe Chimique de France, 1985 , # 5 p. 980 - 998
反应条件
1: 0.05N H2SO4 / H2O / 5 h / 50 °C 2: 74 percent / triethylamine / -15 deg C, 5h, then 50 deg C, 14 h View Scheme
参考文献
Cristau, Henri-Jean; Viala, Jacques; Christol, Henri
Bulletin de la Societe Chimique de France, 1985 , # 5 p. 980 - 998
反应条件
polyphosphoric acid 10 h; Reflux;
参考文献
Sadykov, E. Kh.; Stankevich; Lobanova; Klimenko
Russian Journal of Organic Chemistry, 2014 , vol. 50, # 2 p. 219 - 224
Zh. Org. Khim., 2014 , vol. 50, # 2 p. 226 - 231,6
反应条件
potassium hydroxide Reflux;
参考文献
Sadykov, E. Kh.; Stankevich; Lobanova; Klimenko
Russian Journal of Organic Chemistry, 2014 , vol. 50, # 2 p. 219 - 224
Zh. Org. Khim., 2014 , vol. 50, # 2 p. 226 - 231,6
