2-苯基锡-2-丙烯-1-醇合成路线 （共 8 条）
反应条件
1: diphenyl diselenide With sodium tetrahydroborate in isopropyl alcohol Inert atmosphere; 2: propargyl alcohol With cerium(III) chloride in isopropyl alcohol T=0°C; 3 h; Inert atmosphereReflux; regioselective reaction;
参考文献
Synthesis, , # 23 art. no. M02509SS, p. 4015 - 4021
反应条件
sodium tetrahydroborate; 1-n-butyl-3-methylimidazolium tetrafluoroborate T=60°C; 6 h;
参考文献
Tetrahedron Letters, , vol. 48, # 45 p. 8011 - 8013
反应条件
potassium carbonate 12 h; Ambient temperature;
参考文献
Synthesis, , # 2 p. 146 - 149
反应条件
[Pt(PPh3)4] in toluene T=80°C; 13 h;
参考文献
Journal of Organometallic Chemistry, , vol. 679, # 2 p. 162 - 172
反应条件
1: diphenyl diselenide With sodium tetrahydroborate in isopropyl alcohol Inert atmosphere; 2: propargyl alcohol With cerium(III) chloride in isopropyl alcohol T=0°C; 3 h; Inert atmosphereReflux; regioselective reaction;
参考文献
Synthesis, , # 23 art. no. M02509SS, p. 4015 - 4021
反应条件
pyridine; palladium diacetate T=100°C; 15 h;
参考文献
Journal of Organic Chemistry, , vol. 70, # 2 p. 696 - 698
反应条件
selenium; magnesium 1.) diethyl ether, 2.) diethyl ether, reflux, 30 min, 3.) diethyl ether, reflux, 2 h; Multistep reaction;
参考文献
Russian Journal of Organic Chemistry, , vol. 29, # 2.1 p. 226 - 228
Zhurnal Organicheskoi Khimii, , vol. 29, # 2 p. 272 - 274
反应条件
hydrogenchloride
Yield given;
参考文献
Nedugov, A. N.; Pavlova, N. N.; Shalimov, A. V.
Russian Journal of Organic Chemistry, 1993 , vol. 29, # 2.1 p. 226 - 228
Zhurnal Organicheskoi Khimii, 1993 , vol. 29, # 2 p. 272 - 274
