N-甲氧基-N-甲基-2,2,2-三氟乙酰胺合成路线 （共 18 条）
反应条件
pyridine in tetrahydrofuran Ambient temperature;
参考文献
Graham, Samuel L.; Scholz, Thomas H.
Journal of Organic Chemistry, 1991 , vol. 56, # 13 p. 4260 - 4263
反应条件
pyridine; trifluoroacetic anhydride in dichloromethane
参考文献
US2004/10020 A1, ;
US 20040010020 A1
反应条件
triethylamine in chloroform 0 deg C, 1 h; RT, 1 h;
参考文献
Shaw, Donald A.; Tuominen, Terrence C.
Synthetic Communications, 1985 , vol. 15, # 14 p. 1291 - 1298
参考文献
Tetrahedron Letters, , vol. 27, # 30 p. 3547 - 3550
反应条件
ammonium chloride in tetrahydrofuran T=-78 - 0°C;
参考文献
Guanti, Giuseppe; Banfi, Luca; Narisano, Enrica
Tetrahedron Letters, 1986 , vol. 27, # 30 p. 3547 - 3550
反应条件
magnesium 1.) Et2O, reflux, 1 h, 2.) 0 deg C, RT, 2 h;
参考文献
Shaw, Donald A.; Tuominen, Terrence C.
Synthetic Communications, 1985 , vol. 15, # 14 p. 1291 - 1298
反应条件
n-butyllithium in tetrahydrofuran; hexane T=-78°C; 2.5 h; Inert atmosphere;
参考文献
Hyster, Todd K.; Ruhl, Kyle E.; Rovis, Tomislav
Journal of the American Chemical Society, 2013 , vol. 135, # 14 p. 5364 - 5367
反应条件
n-butyllithium in tetrahydrofuran; hexane T=-78°C; 2.5 h; Inert atmosphere;
参考文献
Hyster, Todd K.; Ruhl, Kyle E.; Rovis, Tomislav
Journal of the American Chemical Society, 2013 , vol. 135, # 14 p. 5364 - 5367
反应条件
n-butyllithium in tetrahydrofuran; hexane T=-78°C; 2.5 h; Inert atmosphere;
参考文献
Hyster, Todd K.; Ruhl, Kyle E.; Rovis, Tomislav
Journal of the American Chemical Society, 2013 , vol. 135, # 14 p. 5364 - 5367
反应条件
n-butyllithium in tetrahydrofuran; hexane T=-78°C; 2.5 h; Inert atmosphere;
参考文献
Hyster, Todd K.; Ruhl, Kyle E.; Rovis, Tomislav
Journal of the American Chemical Society, 2013 , vol. 135, # 14 p. 5364 - 5367
