3-(苯甲氨基羰基)苯硼酸频哪酯合成路线 (共 4 条)
反应条件
benzotriazol-1-ol; triethylamine in N,N-dimethyl-formamide T=20°C; 48 h; Inert atmosphere;
参考文献
De Simone, Rosa; Bruno, Ines; Riccio, Raffaele; Stadler, Katharina; Bauer, Julia; Schaible, Anja M.; Laufer, Stefan; Werz, Oliver
Bioorganic and Medicinal Chemistry, 2012 , vol. 20, # 16 p. 5012 - 5016
反应条件
1: ethyl acetate / 4 h / Inert atmosphere 2: benzotriazol-1-ol; triethylamine / N,N-dimethyl-formamide / 48 h / 20 °C / Inert atmosphere View Scheme
参考文献
Bioorganic and Medicinal Chemistry, , vol. 20, # 16 p. 5012 - 5016
反应条件
1: ethyl acetate / 4 h / Inert atmosphere 2: benzotriazol-1-ol; triethylamine / N,N-dimethyl-formamide / 48 h / 20 °C / Inert atmosphere View Scheme
参考文献
Bioorganic and Medicinal Chemistry, , vol. 20, # 16 p. 5012 - 5016
反应条件
TPPBr2; triethylamine in chloroform T=-60°C; von Braun degradation; Reflux;
参考文献
Vaccari, Daniele; Davoli, Paolo; Spaggiari, Alberto; Prati, Fabio
Synlett, 2008 , # 9 p. 1317 - 1320