(1S,3S,4R)-对薄荷-8-烯-3-醇合成路线 （共 32 条）
反应条件
triethylaluminum; (R)-2,2'-dihydroxy-1,1'-binaphthyl in hexane; dichloromethane; toluene T=0 - 5°C; 1 h; Inert atmosphere; Product distribution / selectivity;
参考文献
EP2279992 A1, ;
Page/Page column 15 ;
反应条件
potassium hydroxide in methanol T=20°C;
参考文献
Serra, Stefano; Brenna, Elisabetta; Fuganti, Claudio; Maggioni, Francesco
Tetrahedron Asymmetry, 2003 , vol. 14, # 21 p. 3313 - 3319
反应条件
silica gel in dichloromethane 1 h; Yield given. Yields of byproduct given;
参考文献
Journal of Organic Chemistry, , vol. 60, # 13 p. 4146 - 4152
反应条件
Daucus carota root homogenate in phosphate buffer T=20°C; pH=6.5; Title compound not separated from byproducts.;
参考文献
Tetrahedron Asymmetry, , vol. 18, # 6 p. 717 - 723
反应条件
Ir-Beta zeolite; hydrogen in cyclohexane T=25°C; P=11250.9 Torr; 20 h; Product distribution; Further Variations:PressuresSolventsTemperaturestime;
参考文献
Chemical Communications, , # 11 p. 1292 - 1293
反应条件
1: Pseudomonas cepacia lipase / various solvent(s) / 20 °C 2: 2 g / KOH / methanol / 20 °C View Scheme
参考文献
Tetrahedron Asymmetry, , vol. 14, # 21 p. 3313 - 3319
反应条件
acetate buffer pH 5.49; sodium lauryl sulfate in water T=20°C; 96 h; dependence on buffer, solvent; Rate constantProduct distribution;
参考文献
Journal of Organic Chemistry, , vol. 49, # 23 p. 4557 - 4559
反应条件
1: trifluoroacetic acid; 5 palladium on barium sulphate; (2R)-2-[bis(4-tert-butylphenyl)methyl]pyrrolidine / #tert!-butyl alcohol / 21 h / 40 °C / 750.08 Torr 2: 0 - 5 °C View Scheme
反应条件
ammonium hydroxide; hexane; sodium T=0 - 3°C;
参考文献
Bulletin of the Agricultural Chemical Society of Japan, , vol. 24, p. 655
