(3S)-3-甲基-1,4-苯并二氮杂卓-2,5-二酮合成路线 （共 5 条）
反应条件
in pyridine 16 h; Heating;
参考文献
Clark, Rachel L.; Carter, Katharine C.; Mullen, Alexander B.; Coxon, Geoffrey D.; Owusu-Dapaah, George; McFarlane, Emma; Duong Thi, M. Dao; Grant, M. Helen; Tettey, Justice N.A.; Mackay, Simon P.
Bioorganic and Medicinal Chemistry Letters, 2007 , vol. 17, # 3 p. 624 - 627
反应条件
1: Et3N / tetrahydrofuran / 20 °C 2: 75 percent / sodium iodide; acetic acid / 12 h / Heating View Scheme
参考文献
Tetrahedron Letters, , vol. 45, # 44 p. 8187 - 8190
参考文献
Bioorganic and Medicinal Chemistry Letters, , vol. 14, # 10 p. 2603 - 2607
反应条件
1: pyridine / 24 h / Heating 2: acetic acid / 24 h View Scheme
参考文献
Bioorganic and Medicinal Chemistry Letters, , vol. 14, # 10 p. 2603 - 2607
反应条件
hydrogenchloride; 4-(N,N-dimethlyamino)pyridine; dicyclohexyl-carbodiimide 1.) 2 h, 0 deg C; 4 h, room temp., 2.) DMF, 4 h, 60 deg C; Yield given. Multistep reaction;
参考文献
Tetrahedron, , vol. 50, # 30 p. 9051 - 9060
