2-甲基-3-氧代-3-苯基丙酸乙酯合成路线 （共 76 条）
参考文献
Simonis; Wojack
Chemische Berichte, 1937 , vol. 70, p. 1837,1846
反应条件
1: 0.5 N aq. sodium hydroxide / 1.) ice-cooling, 3 h, 2.) r.t., 12 h
2: 82 percent / conc. sulfuric acid / 1.) ice-cooling, 3 h, 2.) 0 deg C, 12 h
View Scheme
参考文献
Sato, Masayuki; Ogasawara, Hiromichi; Oi, Keiichi; Kato, Tetsuzo
Chemical & Pharmaceutical Bulletin, 1983 , vol. 31, # 6 p. 1896 - 1901
反应条件
1: 1.) NaH, 60percent in oil / 1.) DMSO, until homogeneous; 2.) DMSO, overnight
2: 63 percent Chromat. / (Bu3Sn)2 / cyclohexane / 36 h / Irradiation
View Scheme
参考文献
Best, Wayne M.; Cook, Anthony P. F.; Russell, James J.; Widdowson, David A.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1986 , p. 1139 - 1144
反应条件
p-NO2-benzenesulfonyl azide; triethylamine in dichloromethane
T=0 - 20°C; Substitution;
参考文献
Benati, Luisa; Nanni, Daniele; Spagnolo, Piero
Journal of Organic Chemistry, 1999 , vol. 64, # 14 p. 5132 - 5138
参考文献
Schmidt,J.; Dieterle
Justus Liebigs Annalen der Chemie, 1910 , vol. 377, p. 53 Anm.
Full Text Show Details
Schmidt; Aeckerle
Justus Liebigs Annalen der Chemie, 1913 , vol. 398, p. 253
参考文献
Meyer,R.; Toegel
Justus Liebigs Annalen der Chemie, 1906 , vol. 347, p. 80
