2,3-二氢-2,2-二甲基茚-1-酮合成路线 （共 46 条）
反应条件
aluminium trichloride
T=24 - 27°C;
参考文献
Bruson,H.A.; Plant,H.L.
Journal of Organic Chemistry, 1967 , vol. 32, p. 3356 - 3362
反应条件
aluminium trichloride
T=24 - 27°C;
参考文献
Bruson,H.A.; Plant,H.L.
Journal of Organic Chemistry, 1967 , vol. 32, p. 3356 - 3362
反应条件
aluminium trichloride
T=24 - 27°C;
参考文献
Bruson,H.A.; Plant,H.L.
Journal of Organic Chemistry, 1967 , vol. 32, p. 3356 - 3362
反应条件
aluminium trichloride
T=21 - 24°C;
参考文献
Bruson,H.A.; Plant,H.L.
Journal of Organic Chemistry, 1967 , vol. 32, p. 3356 - 3362
反应条件
aluminium trichloride
T=19 - 20°C; 3.5 h;
参考文献
Bruson,H.A.; Plant,H.L.
Journal of Organic Chemistry, 1967 , vol. 32, p. 3356 - 3362
反应条件
1: Bu3SnH; AIBN / toluene / 7 h / Heating
2: hydrolysis
View Scheme
参考文献
Bowman; Bridge; Brookes
Tetrahedron Letters, 2000 , vol. 41, # 46 p. 8989 - 8994
反应条件
1: 1.) LDA / 1.) ether, -78 deg C, 30 min, 2.) reflux, 2 d
2: thionyl chloride
3: 16.2 g / AlCl3 / CS2 / 0.5 h / Heating
View Scheme
参考文献
Shimizu, Nobujiro; Osajima, Erika; Tsuno, Yuho
Bulletin of the Chemical Society of Japan, 1991 , vol. 64, # 4 p. 1145 - 1152
反应条件
potassium tert-butylate in diethyl ether; tert-butyl alcohol
Heating;
参考文献
Nishio, Takehiko; Okuda, Norikazu; Kashima, Choji
Liebigs Annales, 1996 , # 1 p. 117 - 120
反应条件
1: NaBH4; CeCl3
2: NaH / dimethylsulfoxide
View Scheme
参考文献
Pincock; Young
Canadian Journal of Chemistry, 2003 , vol. 81, # 10 p. 1083 - 1095
反应条件
1.1: magnesium; ethylene dibromide / tetrahydrofuran / 0 - 20 °C / |Inert atmosphere
1.2: 0 °C / |Inert atmosphere; |Reflux
1.3: 0 °C / |Inert atmosphere
2.1: It-Bu2; bis(1,5-cyclooctadiene)nickel (0) / 1,3,5-trimethyl-benzene / 6 h / 130 °C / |Inert atmosphere
View Scheme
参考文献
Hoshimoto, Yoichi; Hayashi, Yukari; Suzuki, Haruka; Ohashi, Masato; Ogoshi, Sensuke
Angewandte Chemie - International Edition, 2012 , vol. 51, # 43 p. 10812 - 10815
Angew. Chem., 2012 , vol. 124, # 43 p. 10970 - 10973,4
