3-(3,4-二甲氧基苯基)-1-(2-羟基-4,6-二甲氧基苯基)-2-丙烯-1-酮合成路线 （共 27 条）
反应条件
potassium hydroxide in methanol T=20°C; Claisen condensation; 24 h;
参考文献
Singh, Om V.; Muthukrishnan; Sunderavadivelu
Indian Journal of Chemistry - Section B Organic and Medicinal Chemistry, 2005 , vol. 44, # 12 p. 2575 - 2581
反应条件
boron tribromide in dichloromethane T=0°C; 0.5 h;
参考文献
Chu, Han-Wei; Wu, Huan-Ting; Lee, Yean-Jang
Tetrahedron, 2004 , vol. 60, # 11 p. 2647 - 2655
反应条件
1: 99 percent / KOH / ethanol / 3 h / 20 °C 2: 90 percent / BBr3 / CH2Cl2 / 0.5 h / 0 °C View Scheme
参考文献
Chu, Han-Wei; Wu, Huan-Ting; Lee, Yean-Jang
Tetrahedron, 2004 , vol. 60, # 11 p. 2647 - 2655
反应条件
1: 99 percent / KOH / ethanol / 3 h / 20 °C 2: 90 percent / BBr3 / CH2Cl2 / 0.5 h / 0 °C View Scheme
参考文献
Chu, Han-Wei; Wu, Huan-Ting; Lee, Yean-Jang
Tetrahedron, 2004 , vol. 60, # 11 p. 2647 - 2655
反应条件
1: 65 percent / dimethyl dioxirane / acetone; CH2Cl2 / 1 h / 0 - 20 °C 2: 95 percent / K2CO3 / acetone / 6 h / Heating 3: 71 percent / I2; pyridine / 8 h / Heating 4: 94 percent / BBr3 / CH2Cl2 / 0.5 h / 0 °C 5: 90 percent / dimethyl dioxirane / acetone; CH2Cl2 / 0.33 h / 0 - 20 °C 6: 87 percent / K2CO3 / acetone; CH2Cl2 / 6 h / Heating View Scheme
参考文献
Tetrahedron, , vol. 60, # 11 p. 2647 - 2655
反应条件
oxygen; methylene blue in methanol; benzene 48 h; Irradiation;
参考文献
Sharma, Anil; Chibber, S. S.; Chawla, H. M.
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, 1980 , vol. 19, # 10 p. 905 - 906
反应条件
oxygen; methylene blue in benzene 48 h; Irradiation;
参考文献
Sharma, Anil; Chibber, S. S.; Chawla, H. M.
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, 1980 , vol. 19, # 10 p. 905 - 906
反应条件
iodine in dimethyl sulfoxide T=150°C; 0.5 h; Inert atmosphere;
参考文献
Deodhar, Mandar; Wood, Kasey; Black, David Stclair; Kumar, Naresh
Australian Journal of Chemistry, 2012 , vol. 65, # 10 p. 1377 - 1383,7
反应条件
tris(4-bromophenyl)amine; lithium perchlorate in methanol; dichloromethane electrolysis 2 F/mol;
参考文献
Tetrahedron Letters, , vol. 27, # 3 p. 407 - 408
反应条件
tris(4-bromophenyl)amine; lithium perchlorate in methanol; dichloromethane electrolysis 4 F/mol;
参考文献
Tetrahedron Letters, , vol. 27, # 3 p. 407 - 408
