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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
10496-72-7
合成路线
（共 14 条）
98-85-1
DL-1-苯乙醇
+
105-13-5
茴香醇
→
反应条件
1669-49-4
3-(4-甲氧基苯基)苯丙酮
+
10496-72-7
反应条件
tris-(dibenzylideneacetone)dipalladium(0); CsOH; 2,6-bis(N-butyl-N'-methylenebenzimidazolium)-1-bromophenylene dibromide in para-xylene T=125°C; Inert atmosphere;
参考文献
Kose, Osamu; Saito, Susumu
Organic and Biomolecular Chemistry, 2010 , vol. 8, # 4 p. 896 - 900
959-33-1
4-甲氧基查耳酮
→
反应条件
10496-72-7
反应条件
[IrH(1,5-cyclooctadiene)Cl(HCN(i-Pr)CHCN(C2H4PPh2))]PF6; isopropyl alcohol; potassium hydroxide 4 h; Inert atmosphere;
参考文献
Gong, Xue; Zhang, Hong; Li, Xingwei
Tetrahedron Letters, 2011 , vol. 52, # 43 p. 5596 - 5600
98-85-1
DL-1-苯乙醇
+
105-13-5
茴香醇
→
反应条件
10496-72-7
反应条件
potassium hydroxide; cis-[RuCl2(dimethylsulfoxide-S)3(dimethylsulfoxide-O)] in 1,4-dioxane T=80°C; 168 h;
参考文献
Satyanarayana, Ponnam; Reddy, Ganapam Manohar; Maheswaran, Hariharasharma; Kantam, Mannepalli Lakshmi
Advanced Synthesis and Catalysis, 2013 , vol. 355, # 9 p. 1859 - 1867
109643-11-0
→
反应条件
10496-72-7
反应条件
hydrogen; palladium-copper; silica gel in ethanol T=25°C; P=760 Torr; Kinetics;
参考文献
Spee; Boersma; Meijer; Slagt; Van Koten; Geus
Journal of Organic Chemistry, 2001 , vol. 66, # 5 p. 1647 - 1656
98-86-2
苯乙酮
+
105-13-5
茴香醇
→
反应条件
10496-72-7
反应条件
1,4-diaza-bicyclo[2.2.2]octane; rhodium(III) acetylacetonate; potassium hydroxide in toluene T=110°C; 4 h; Sealed tube; Reagent/catalyst;
参考文献
Satyanarayana, Ponnam; Reddy, Ganapam Manohar; Maheswaran, Hariharasharma; Kantam, Mannepalli Lakshmi
Advanced Synthesis and Catalysis, 2013 , vol. 355, # 9 p. 1859 - 1867
98-85-1
DL-1-苯乙醇
+
123-11-5
大茴香醛
→
反应条件
1669-49-4
3-(4-甲氧基苯基)苯丙酮
+
10496-72-7
反应条件
tris(triphenylphosphine)ruthenium(II) chloride; potassium hydroxide in 1,4-dioxane T=80°C; 40 h;
参考文献
Cho, Chan Sik; Kim, Bok Tae; Yoon, Nam Sik
Applied Organometallic Chemistry, 2011 , vol. 25, # 9 p. 695 - 698
959-33-1
4-甲氧基查耳酮
→
反应条件
3906-07-8
+
1669-49-4
3-(4-甲氧基苯基)苯丙酮
+
10496-72-7
反应条件
hydrogen; bis-(ethyl)-phenyl-phosphine; [Ir2(OMe)2(1,5-cyclooctadiene)2] in toluene T=100°C; P=15200 Torr; 24 h; regioselectivity; other phenyl substituted enones; Product distribution;
参考文献
Spogliarich; Farnetti; Graziani
Tetrahedron, 1991 , vol. 47, # 10-11 p. 1965 - 1976
1669-49-4
3-(4-甲氧基苯基)苯丙酮
→
反应条件
10496-72-7
反应条件
lithium aluminium tetrahydride
参考文献
De Puy; Leary
Journal of the American Chemical Society, 1957 , vol. 79, p. 3705,3708
959-33-1
4-甲氧基查耳酮
→
反应条件
1669-49-4
3-(4-甲氧基苯基)苯丙酮
+
10496-72-7
反应条件
sodium formate in water T=100°C; 12 h; chemoselective reaction;
参考文献
Bagal, Dattatraya B.; Qureshi, Ziyauddin S.; Dhake, Kishor P.; Khan, Shoeb R.; Bhanage, Bhalchandra M.
Green Chemistry, 2011 , vol. 13, # 6 p. 1490 - 1494
22252-15-9
(E)-3-(4-甲氧基苯基)-1-苯基-丙-2-烯-1-酮
→
反应条件
10496-72-7
反应条件
lithium aluminium tetrahydride; aluminium trichloride in diethyl ether
参考文献
Hase,T.
Acta Chemica Scandinavica (1947-1973), 1969 , vol. 23, p. 2403 - 2408
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