2-氯-6-甲酰基-苯甲酸乙酯合成路线 （共 3 条）
反应条件
hydrogenchloride in tetrahydrofuran; water 4 h; Reflux;
参考文献
Aksjonova, Kristine; Belyakov, Sergey; Liepinsh, Edvards; Boman, Arne; Lundstedt, Torbjorn; Lek, Per; Trapencieris, Peteris
Synthesis (Germany), 2012 , vol. 44, # 14 art. no. SS-2012-N0094-OP, p. 2200 - 2208
反应条件
1.1: n-butyllithium / tetrahydrofuran; hexane / 0.75 h / -78 °C / Inert atmosphere 1.2: -78 - -20 °C / Inert atmosphere 2.1: hydrogenchloride / tetrahydrofuran; water / 4 h / Reflux View Scheme
参考文献
Aksjonova, Kristine; Belyakov, Sergey; Liepinsh, Edvards; Boman, Arne; Lundstedt, Torbjorn; Lek, Per; Trapencieris, Peteris
Synthesis (Germany), 2012 , vol. 44, # 14 art. no. SS-2012-N0094-OP, p. 2200 - 2208
反应条件
1.1: toluene-4-sulfonic acid / toluene / 14 h / Reflux; Inert atmosphere 2.1: n-butyllithium / tetrahydrofuran; hexane / 0.75 h / -78 °C / Inert atmosphere 2.2: -78 - -20 °C / Inert atmosphere 3.1: hydrogenchloride / tetrahydrofuran; water / 4 h / Reflux View Scheme
参考文献
Aksjonova, Kristine; Belyakov, Sergey; Liepinsh, Edvards; Boman, Arne; Lundstedt, Torbjorn; Lek, Per; Trapencieris, Peteris
Synthesis (Germany), 2012 , vol. 44, # 14 art. no. SS-2012-N0094-OP, p. 2200 - 2208
