反应条件
1.1: N-bromosuccinmide; meta-chloroperoxybenzoic acid / tetrachloromethane / 6 h / 80 °C
2.1: N,N-dimethyl-formamide / 10 h / 160 °C / Inert atmosphere
3.1: dichloromethane; water / -15 °C / Inert atmosphere
3.2: 20 °C / Inert atmosphere
View Scheme
参考文献
Gao, Weiqiang; Yan, Mei; Ge, Shenguang; Liu, Xiaoxia; Yu, Jinghua
Spectrochimica Acta - Part A: Molecular and Biomolecular Spectroscopy, 2012 , vol. 95, p. 218 - 223