1: methanol / 20 °C / Inert atmosphere 2: sodium tetrahydroborate / methanol / 4 h / 20 °C / Inert atmosphere 3: lithium aluminium tetrahydride / tetrahydrofuran; diethyl ether / 0 °C / Reflux View Scheme
参考文献
Larkin, Joseph D.; Frimat, Karine A.; Fyles, Thomas M.; Flower, Stephen E.; James, Tony D.
New Journal of Chemistry, 2010 , vol. 34, # 12 p. 2922 - 2931
1.1: 50 percent / TFA / 0.08 h 2.1: DIBAL-H / CH2Cl2; hexane / 3 h / 20 °C 2.2: 47 percent / NH4Cl / H2O / 2 h View Scheme
参考文献
Rao, Polisetti Dharma; Dhanalekshmi, Savithri; Littler, Benjamin J.; Lindsey, Jonathan S.
Journal of Organic Chemistry, 2000 , vol. 65, # 22 p. 7323 - 7344
1: 2-methoxybromobenzene With magnesium in tetrahydrofuran Heating; 2: [4-cyanophenyl]methanone in tetrahydrofuran T=0 - 20°C; 3 h; 3: With dipyridinium dichromate; 4 A molecular sieve in dichloromethane T=20°C; 2 h; Further stages.;
