1: 95 percent / phosphorus tribromide / CH2Cl2 / 12 h / 0 °C 2: toluene / 6 h / Heating View Scheme
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1: (4-methoxyphenyl)methanol With trifluoromethylsulfonic anhydride; bis-(phenyl)-sulfoxide; N,N,N',N'-tetra-methylnaphthalene-1,8-diamine in toluene T=-78°C; 2: sodium salt of dimethylmalonate in tetrahydrofuran; toluene T=-78 - 20°C;
参考文献
Takuwa, Tomofumi; Minowa, Tomofumi; Fujisawa, Hidehiko; Mukaiyama, Teruaki
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1: (4-methoxyphenyl)methanol With n-butyllithium; chloro-diphenylphosphine 2: cyclohexanol With 2,3,5,6-tetrafluoro-1,4-benzoquinone in dichloromethane T=20°C; 3 h;
