1: With sodium in ethanol
T=0°C; 2 h; Inert atmosphere;
2: With sodium hydroxide in ethanol; water
T=0°C; 4 h; Inert atmosphere;
3: With hydrogenchloride; potassium dihydrogen ortho-phosphate in water
T=20°C; pH=3.5; 12 h; Inert atmosphere;
参考文献
Zhao, Peng; Beaudry, Christopher M.
Organic Letters, 2013 , vol. 15, # 2 p. 402 - 405
1: With potassium tert-butylate in tetrahydrofuran
T=-50 - 20°C; 0.5 h;
2: With water in tetrahydrofuran
T=20°C; 4 h;
3: With hydrogenchloride
T=100°C; Further stages.;
参考文献
Achmatowicz, Michal; Thiel, Oliver R.; Gorins, Gilles; Goldstein, Corinne; Affouard, Caroline; Jensen, Randy; Larsen, Robert D.
Journal of Organic Chemistry, 2008 , vol. 73, # 17 p. 6793 - 6799
