反应条件
1: acetoacetic acid methyl ester With 1,8-diazabicyclo[5.4.0]undec-7-ene; sodium iodide in N,N-dimethyl-formamide T=20°C; 0.25 h; 2: 1,10-bis-bromodecane in N,N-dimethyl-formamide T=20°C; 2 h; 3: With sodium hydroxide in water T=20 - 60°C; 5 h;
参考文献
Tanabe, Yoo; Matsumoto, Noriaki; Higashi, Takahiro; Misaki, Tomonori; Itoh, Tomotaka; Yamamoto, Misako; Mitarai, Kumi; Nishii, Yoshinori
Tetrahedron, 2002 , vol. 58, # 41 p. 8269 - 8280
