1,3,5,7-tetra-azatricyclo[5.1.1.13,5]decane in cyclohexane
Heating;
参考文献
Ribeiro, Rodrigo S.; De Souza, Rodrigo O. M. A.; Vasconcellos, Mario L. A. A.; Oliveira, Bianca L.; Ferreira, Leonardo C.; Aguiar, Lucia C. S.
Synthesis, 2007 , # 1 p. 61 - 64
1: acetoacetic acid methyl ester With sodium hydride in tetrahydrofuran
T=0°C; 0.166667 h;
2: n-butyllithium in tetrahydrofuran; cyclohexane
T=0°C; 0.166667 h;
3: 3-fluoro-1-bromomethylbenzene With hydrogenchloride
more than 3 stages;
参考文献
Chen, Shoujun; Sun, Lijun; McCleary, Joel
Patent: US2003/236302 A1, 2003 ;
Location in patent: Page 11 ;
