1,3-丙酮二羧酸二乙酯合成路线 （共 169 条）
反应条件
sulfuric acid
T=90°C; 0.5 h;
参考文献
Besson, Thierry; Joseph, Benoit; Moreau, Pascale; Viaud, Marie-Claude; Coudert, Gerard; Guillaumet, Gerald
Heterocycles, 1992 , vol. 34, # 2 p. 273 - 291
反应条件
acetic anhydride in acetic acid
8 h; Heating;
参考文献
Ahmed,S. et al.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1976 , p. 1969 - 1975
反应条件
1: 85 percent / Et3N, anhyd. MgCl2 / benzene / Heating
2: 30.1 percent / 3 h / 180 °C
View Scheme
参考文献
Yamato, Masatoshi; Kusunoki, Youichiro
Chemical & Pharmaceutical Bulletin, 1981 , vol. 29, # 5 p. 1214 - 1220
参考文献
Asahina; Nogami
Yakugaku Zasshi, 1941 , vol. 61, p. 51,54
Bulletin of the Chemical Society of Japan, 1942 , vol. 17, p. 221,223
参考文献
Yamato, Masatoshi; Kusunoki, Youichiro
Chemical & Pharmaceutical Bulletin, 1981 , vol. 29, # 5 p. 1214 - 1220
反应条件
sodium hydroxide
T=35°C; 24 h; pH= 9-10;
参考文献
Schneller, Stewart W.; Luo, Jiann-Kuan; Hosmane, Ramachandra S.; Duerrfeld, Rainer H.
Journal of Heterocyclic Chemistry, 1984 , vol. 21, p. 1153 - 1155
参考文献
Stahly, G. P.; Marlett, E. M.; Nelson, G. E.
Journal of Organic Chemistry, 1983 , vol. 48, # 23 p. 4423 - 4426
反应条件
sulfuric acid in ethanol; benzene
1080 h; Heating;
参考文献
Dietz, Timothy M.; Trebra, Robert J. von; Swanson, Barry J.; Koch, Tad H.
Journal of the American Chemical Society, 1987 , vol. 109, # 6 p. 1793 - 1797
反应条件
iodine in ethanol
cyclocondensation; Heating;
参考文献
Rangnekar, Dinesh W.; Kazemi, Gadhir J.; Malanker, Jayesh V.; Ramamurthy, Rajesh
Phosphorus, Sulfur and Silicon and Related Elements, 1998 , vol. 141, p. 185 - 190
反应条件
sulfuryl dichloride
Erwaermen des Reaktionsprodukts mit Thioharnstoff in Aethanol;
参考文献
Sprague; Lincoln; Ziegler
Journal of the American Chemical Society, 1946 , vol. 68, p. 268
