barium dihydroxide; Na2[PdCl4] in N,N-dimethyl acetamide T=100°C; 14 h;
参考文献
Aramendia, Maria A.; Borau, Victoriano; Jimenez, Cesar; Marinas, Jose M.; Ruiz, Jose R.; Urbano, Francisco J.
Tetrahedron Letters, 2002 , vol. 43, # 15 p. 2847 - 2849
barium dihydroxide; Na2[PdCl4] in N,N-dimethyl acetamide T=100°C; 14 h;
参考文献
Aramendia, Maria A.; Borau, Victoriano; Jimenez, Cesar; Marinas, Jose M.; Ruiz, Jose R.; Urbano, Francisco J.
Tetrahedron Letters, 2002 , vol. 43, # 15 p. 2847 - 2849
potassium hydroxide; iodine in diethyl ether; dimethyl sulfoxide addn. of C6H5CH(COOC2H5)2 to mixt. of Cr(CO)3-complex/powd. KOH in DMSO (stirring; 20°C, 6 h), diln. with aq. HCl, extn. with Et2O, treating with excess I2 (room temp., 3 h); distn. (reduced pressure); identification by GC and NMR;
