Jae, Hwan-Soo; Winn, Martin; Dixon, Douglas B.; Marsh, Kennan C.; Nguyen, Bach; Opgenorth, Terry J.; Von Geldern, Thomas W.
Journal of Medicinal Chemistry, 1997 , vol. 40, # 20 p. 3217 - 3227
in tetrahydrofuran; diethyl ether; pentane
a) -110 deg C, 2 h, b) to r.t.;
参考文献
Seyferth, Dietmar; Weinstein, Robert M.; Hui, Richard C.; Wang, Wei-Liang; Archer, Colin M.
Journal of Organic Chemistry, 1991 , vol. 56, # 20 p. 5768 - 5773
in further solvent(s)
Kinetics; byproducts: C2H5F, (C2H5)2O, OPF2(OC2H5); thermal decomposition of LiPF6 soln. in diethylcarbonate at 85-100 °C for 1-4 weeks; also OPF(OC2H5)2 and C2H4 obtained; detd. by chromy.;
参考文献
Campion, Christopher L.; Li, Wentao; Lucht, Brett L.
Journal of the Electrochemical Society, 2005 , vol. 152, # 12 p. A2327-A2334
Parrott, Andrew J.; Bourne, Richard A.; Gooden, Peter N.; Poliakoff, Martyn; Irvine, Derek J.; Bevinakatti, Han. S.
Organic Process Research and Development, 2010 , vol. 14, # 6 p. 1420 - 1426
